Projects funded by the NCN


Information on the principal investigator and host institution

Information of the project and the call

Keywords

Equipment

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High-performance layer electrochromatography - research on a new separation technique

2016/23/B/ST4/02877

Keywords:

planar elektrochromatography layer elektrochromatography hydrodynamic flow electroosmotic flow simultaneous separation of several samples parallel separation

Descriptors:

  • ST4_6: Instrumental methods in chemistry
  • ST4_8: Organic chemistry

Panel:

ST4 - Chemistry: physical chemistry/chemical physics, theoretical chemistry, analytical chemistry, inorganic chemistry, organic chemistry, method development

Host institution :

Uniwersytet Medyczny w Lublinie, Wydział Farmaceutyczny

woj. lubelskie

Other projects carried out by the institution 

Principal investigator (from the host institution):

prof. Tadeusz Dzido 

Number of co-investigators in the project: 9

Call: OPUS 12 - announced on 2016-09-15

Amount awarded: 988 850 PLN

Project start date (Y-m-d): 2017-08-30

Project end date (Y-m-d): 2022-06-29

Project duration:: 58 months (the same as in the proposal)

Project status: Project settled

Project description

Download the project description in a pdf file

Note - project descriptions were prepared by the authors of the applications themselves and placed in the system in an unchanged form.

Equipment purchased [PL]

  1. Komputer (6 600 PLN)
  2. Siłownik hydrauliczny (8 000 PLN)
  3. Ultratermostat (15 000 PLN)
  4. Cela przepływowa do detektora UV-VIS (6 szt.) (31 200 PLN)
  5. Komora, i jej modyfikacje na płytki chromatograficzne o wymiarach 10x10, 10x20 cm z obudową bezpieczeństwa, do wysokosprawnej elektrochromatogra fii warstwowej (80 000 PLN)
  6. Kontrolery cyfrowe do zasilacza wysokonapieciowego.
  7. Detektor UV-VIS (6 szt.) (132 000 PLN)
  8. Pompa wysokociśnieniowa do chromatografii cieczowej gradientowej (55 000 PLN)
  9. Zasilacz wysokonapięciowy prądu stałego (20 000 PLN)
  10. Oprogramowanie do pomp chromatograficznych, detektorów, dozowanika automatycznego i zaworu sześciodrożnego (33 000 PLN)
  11. Automatyczny podajnik próbek (autosampler) (70 000 PLN)
  12. Pompa cieczowa wysokociśnieniowa (20 000 PLN)

Information in the final report

  • Publication in academic press/journals (4)
  1. An underestimated technique. Does pressurized and pressure-assisted capillary electrochromatography have potential in drug and pharmacological-active compounds analysis?
    Authors:
    MICHAŁ ŻMUDA-TRZEBIATOWSKI, RADOSŁAW Ł. GWARDA, TADEUSZ H. DZIDO
    Academic press:
    Curr. Iss. Pharm. Med. Sci. (rok: 2019, tom: 32, strony: 92-98), Wydawca: Sciendo
    Status:
    Published
    DOI:
    10.2478/cipms-2019-0018 - link to the publication
  2. High performance (high pressure) layer electrochromatography separation technique: equipment and preliminary results
    Authors:
    Radosław Łukasz Gwarda, Tadeusz Henryk Dzido.
    Academic press:
    Analytical Chemistry (rok: 2022, tom: 94, strony: 9091-9096), Wydawca: ACS
    Status:
    Published
    DOI:
    10.1021/acs.analchem.2c01376 - link to the publication
  3. Comparison of overpressured-layer chromatography and high-performance/high-pressure layer electrochromatography using the new prototype equipment in various operational modes
    Authors:
    Radosław Łukasz Gwarda, Tadeusz Henryk Dzido
    Academic press:
    Molecules (rok: 2022, tom: 27, strony: 4032), Wydawca: MDPI
    Status:
    Published
    DOI:
    10.3390/molecules27134032 - link to the publication
  4. Differences in the efficiency of separation of analgesic drugs by high-performance thin-layer chromatography with similar octadecyl silica-based adsorbents.
    Authors:
    MICHAŁ ŻMUDA TRZEBIATOWSKI, RADOSŁAW Ł. GWARDA, TADEUSZ H. DZIDO
    Academic press:
    Journal of Planar Chromatography (rok: 2019, tom: 32, strony: 517-520), Wydawca: Akademiai Kiado, Budapeszt, Węgry
    Status:
    Published
    DOI:
    10.1556/1006.2019.32.6.11 - link to the publication