Projects funded by the NCN

Information on the principal investigator and host institution

Information of the project and the call

Keywords

Equipment

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Future prospectives of spectrochemical solid and liquid sample analysis in bioinorganic trace and speciation analysis: from macro to microanalytics

2012/06/A/ST4/00382

Keywords:

sample destruction techniques optical emission and absorption spectrometry capillary electrophoresis bioinorganic speciation analysis lab-on-a-chip technology trace analysis microsampling techniques certified reference materials real samples hyphenated techniques microwave macro and microplasmas green analytical chemistry

Descriptors:

  • ST4_3: Molecular architecture and structure
  • ST4_6: Instrumental methods in chemistry
  • ST4_8: Organic chemistry

Panel:

ST4 - Chemistry: physical chemistry/chemical physics, theoretical chemistry, analytical chemistry, inorganic chemistry, organic chemistry, method development

Host institution :

Politechnika Poznańska, Wydział Technologii Chemicznej

woj. wielkopolskie

Other projects carried out by the institution 

Principal investigator (from the host institution):

prof. Henryk Matusiewicz 

Number of co-investigators in the project: 6

Call: MAESTRO 3 - announced on 2012-06-15

Amount awarded: 1 795 150 PLN

Project start date (Y-m-d): 2013-04-18

Project end date (Y-m-d): 2016-10-17

Project duration:: 42 months (the same as in the proposal)

Project status: Project settled

Equipment purchased [PL]

  1. Cieczowy mikroreaktor chemiczny (2 szt.) (30 000 PLN)
  2. System ekstrakcyjny cząstek stałych (SPX) (70 000 PLN)
  3. Elektromagnetyczny indukcyjny reaktor chemiczny (2 szt.) (40 000 PLN)
  4. Miniaturowe systemy analityczne: mikro-chip mikrofalowa plazma, mikro-chip elektroforeza kapilarna, mikro-rozpylacz ultradźwiękowy (3 szt.) (60 000 PLN)
  5. Miniaturowy optyczny CCD spektrometr emisyjny (50 000 PLN)
  6. System laserowego odparowania (LA) (500 000 PLN)
  7. Wnęka mikrofalowa pola magnetycznego, wnęka mikrofalowa z plazmą rotacyjną (2 szt.) (60 000 PLN)
  8. Zestaw do wprowadzania próbek.
  9. Miniaturowy system modułowy: pompa ciśnieniowa, miernik przepływu mikrolitowych objętości cieczy, chip mikroprzepływowy (3 szt.) (48 406 PLN)
  10. Antywibracyjny stół aparaturowy (4 723 PLN)
  11. Spektrofluorymetr (100 000 PLN)

Information in the final report

  • Publication in academic press/journals (17)
  1. Analytical evaluation of a quadruple-mode micro-flow ultrasonic nebulizer for sample introduction in microwave induced plasma spectrometry
    Authors:
    H. Matusiewicz, M. Ślachciński
    Academic press:
    Microchemical Journal (rok: 2017, tom: 130, strony: 345-352), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.010 - link to the publication
  2. Pressurized flow solubilization system using electromagnetic induction heating technique for simultaneous determination of inorganic elements (Ba, Ca, Cd, Cu, Fe, Mg, Mn, Na, Pb, Sr, Zn) in sonicate slurries of biological materials by microwave induced plasma optical emission spectrometry (MIP-OES)
    Authors:
    H. Matusiewicz, M. Ślachciński
    Academic press:
    Journal of the Brazilian Chemical Society (rok: 2016, tom: 27, strony: 584-590), Wydawca: Sociedade Brasileira de Quimica
    Status:
    Published
    DOI:
    10.5935/0103-5053.20150294 - link to the publication
  3. Sample Preparation for Inorganic Trace Element Analysis
    Authors:
    Henryk Matusiewicz
    Academic press:
    Physical Sciences Reviews (rok: 2017, tom: 2, strony: 20455), Wydawca: De Gruyter
    Status:
    Published
    DOI:
    10.1515/psr-2017-8001 - link to the publication
  4. Sequential multi-element determination of iron and zinc in water samples by high-resolution continuum source graphite furnace atomic absoprtion spectrometry after column solid-phase extraction onto multiwalled carbon nanotubes
    Authors:
    M. Krawczyk, M. Jeszka-Skowron, H. Matusiewicz
    Academic press:
    Microchemical Journal (rok: 2014, tom: 117, strony: 138-143), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.microc.2014.06.023 - link to the publication
  5. Ultrasonic nebulization, multimode sample introduction system for simultaneous determination of hydride-forming, cold vapor, and non-hydride-forming elements by microwave-induced plasma spectrometry
    Authors:
    H. Matusiewicz, M. Ślachciński
    Academic press:
    Spectroscopy Letters (rok: 2014, tom: 47, strony: 415-426), Wydawca: Taylor&Francis
    Status:
    Published
    DOI:
    10.2013.804421 - link to the publication
  6. Development of interface for online coupling of micro-fluidic chip-based photo-micro-reactor/ultrasonic nebulization with microwave induced plasma spectrometry and its application in simultaneous determination of inorganic trace elements in biological materials
    Authors:
    H. Matusiewicz, M. Ślachciński
    Academic press:
    Microchemical Journal (rok: 2015, tom: 119, strony: 133-139), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.microc.2014.11.009 - link to the publication
  7. Potential release of in vivo trace metals from metallic medical implants in the human body: From ion to nanoparticles - A systematic analytical review
    Authors:
    H. Matusiewicz
    Academic press:
    Acta Biomaterialia (rok: 2014, tom: 14, strony: 2379-2403), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.actbio.2014.02.027 - link to the publication
  8. Recent achievements in sample introduction systems for use in chemical vapor generation plasma optical emission and mass spectrometry: From macro- to microanalytics
    Authors:
    M. Ślachciński
    Academic press:
    Applied Spectroscopy Reviews (rok: 2014, tom: 49, strony: 271-321), Wydawca: Taylor&Francis
    Status:
    Published
    DOI:
    10.1080/05704928.2013.823547 - link to the publication
  9. Solid-phase extraction with multiwalled carbonnanotubes prior to photochemical generation of cadmium coupled to high-resolution continuum source atomic absorption spectrometry
    Authors:
    E. Stanisz, M. Krawczyk, H. Matusiewicz
    Academic press:
    J. Anal. At. Spectrom (rok: 2014, tom: 29, strony: 2388–2397), Wydawca: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/C4JA00278D - link to the publication
  10. Trace determination of Hg together with As, Sb, Se by miniaturized optical emission spectrometry integrated with chemical vapor generation and capacitively coupled argon microwave miniplasma discharge
    Authors:
    H. Matusiewicz, M. Ślachciński
    Academic press:
    Spectrochimica Acta Part B (rok: 2017, tom: 133, strony: 52–59), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.sab.2017.04.010 - link to the publication
  11. A Comparison of Electrothermal Vaporization and Laser Ablation for the Determination of Trace Elements in Solid Samples by Microwave Induced Plasma Optical Emission Spectrometry
    Authors:
    Henryk Matusiewicz and Mariusz Ślachciński
    Academic press:
    Ecological Chemistry and Engineering S (rok: 2018, tom: 25 (2), strony: 45315), Wydawca: DE GRUYTER OPEN
    Status:
    Accepted for publication
    DOI:
    brak - link to the publication
  12. Generation of volatile copper species after in situ ionic liquid formation dispersive liquid-liquid microextraction prior to atomic absorption spectrometric detection
    Authors:
    E. Stanisz, A. Zgoła-Grześkowiak, H. Matusiewicz
    Academic press:
    Talanta (rok: 2014, tom: 129, strony: 254-262), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.talanta.2014.05.048 - link to the publication
  13. Simultaneous determination of As, Bi, Sb, Se and Sn by microwave induced plasma spectrometry using a quadruple-mode microflow ultrasonic nebulizer for in situ hydride generation with internal standardization
    Authors:
    H. Matusiewicz, M. Slachciński
    Academic press:
    Microchemical Journal (rok: 2017, tom: Volume 131, strony: 70–78), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.microc.2016.11.017 - link to the publication
  14. Ultrasonic nebulization/UV photolysis vapor generation sample introduction system for the determination of conventional hydride (As,Bi,Sb,Se,Sn) and cold vapor (Hg,Cd) generation elements in reference materials in the presence of acetic acid by microwave-induced plasma spectrometry
    Authors:
    H. Matusiewicz, M. Ślachciński
    Academic press:
    Spectroscopy Letters (rok: 2013, tom: 46, strony: 315-326), Wydawca: Taylor&Francis
    Status:
    Published
    DOI:
    10.2012.725702 - link to the publication
  15. Development of a one-step microwave-assisted subcritical water extraction for simultaneous determination of inorganic elements (Ba,Ca,Cu,Fe,Mg,Mn,Na,Pb,Sr,Zn) in reference materials by microwave induced plasma spectrometry
    Authors:
    H. Matusiewicz, M. Slachciński
    Academic press:
    Microchemical Journal (rok: 2014, tom: 115, strony: 45453), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.microc.2014.02.002 - link to the publication
  16. Evaluation of five phase digitally controlled rotating field plasma source for photochemical mercury vapor generation optical emission spectrometry
    Authors:
    H. Matusiewicz, M. Ślachciński, P. Pawłowski, M. Portalski
    Academic press:
    Analytical Sciences (rok: 2015, tom: 31, strony: 987-995), Wydawca: The Japan Society for Analytical Chemistry
    Status:
    Published
    DOI:
    10.2116/analsci.31.987 - link to the publication
  17. Task specific ionic liquid-coated PTFE tube for solid-phase microextraction prior to chemical and photo-induced mercury cold vapour generation
    Authors:
    E. Stanisz, J. Werner, H. Matusiewicz
    Academic press:
    Microchemical Journal (rok: 2014, tom: 114, strony: 229-237), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.microc.2014.01.007 - link to the publication

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