Projects funded by the NCN


Information on the principal investigator and host institution

Information of the project and the call

Keywords

Equipment

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Design and preparation of heterometallic molecular clusters. Studies of their catalytic properties and transformation to novel nanomaterials

2018/29/B/ST5/00341

Keywords:

new materials molecular clusters coordination chemistry catalysis supramolecular chemistry

Descriptors:

  • ST5_8: Metals, alloys
  • ST5_14: Other related subjects
  • ST5_24:

Panel:

ST5 - Materials: materials synthesis, structure-properties relations, advanced and functional materials with designed properties, (macro)molecular architecture, material engineering

Host institution :

Politechnika Wrocławska

woj. dolnośląskie

Other projects carried out by the institution 

Principal investigator (from the host institution):

prof. Piotr Sobota 

Number of co-investigators in the project: 9

Call: OPUS 15 - announced on 2018-03-15

Amount awarded: 1 462 800 PLN

Project start date (Y-m-d): 2019-03-21

Project end date (Y-m-d): 2023-03-20

Project duration:: 48 months (the same as in the proposal)

Project status: Project settled

Project description

Download the project description in a pdf file

Note - project descriptions were prepared by the authors of the applications themselves and placed in the system in an unchanged form.

Equipment purchased [PL]

  1. rotacyjna pompa olejowa (1 880 PLN)
  2. Młynek laboratoryjny 400g (1 957 PLN)
  3. młynek laboratoryjny analityczny (4 341 PLN)
  4. Urządzenie wielofunkcyjne (drukarka kolorowa + skaner) (1 500 PLN)
  5. Zestaw wyparny: wyparka rotacyjna z pompą, kontrolerem próżni, butelką Woulffa (2 szt.) (52 000 PLN)
  6. Recyrkulator chłodzący (15 000 PLN)
  7. mieszadła laboratoryjne cyfrowe z grzaniem 2 sztuki (2 822 PLN)
  8. Mieszadło mechaniczne cyfrowe (3 293 PLN)
  9. Systemu do oczyszczania rozpuszczalników.
  10. Wyparka rotacyjna (17 307 PLN)
  11. Zestaw do napełniania kolumienek do chromatografu flash (35 000 PLN)
  12. przenośne naczynia Dewara o pojemności 2l - 3 sztuki (5 737 PLN)
  13. Komputer (PC) (3 500 PLN)
  14. Mieszadło magnetyczne z grzaniem i czujnikiem temperatury (5 szt.) (21 500 PLN)
  15. Monitor do komputera (1 500 PLN)
  16. Pompa próżniowa membranowa, chemoodporna do wyparki rotacyjnej (5 922 PLN)
  17. Waga laboratoryjna (2 967 PLN)

Information in the final report

  • Publication in academic press/journals (7)
  1. Structural analysis and catalytic activity of tetranuclear metal carboxylate clusters with a [KZn3(l3-OH)(OOCCPh3)6] or [Zn4(l4-O)(OOCCPh3)6] central motif
    Authors:
    Rafał Petrus, Józef Utko and Piotr Sobota
    Academic press:
    New Journal of Chemistry (rok: 2020, tom: 44, strony: 13771), Wydawca: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/d0nj02540b - link to the publication
  2. Heterometallic 3d–4f Alkoxide Precursors for the Synthesis of Binary Oxide Nanomaterials
    Authors:
    Rafał Petrus, Adrian Kowaliński, Józef Utko, Karolina Matuszak, Tadeusz Lis, Piotr Sobota
    Academic press:
    Inorganic Chemistry (rok: 2023, tom: 62(5), strony: 2197–2212), Wydawca: American Chemical Society
    Status:
    Published
    DOI:
    10.1021/acs.inorgchem.2c03872 - link to the publication
  3. Magnesium and zinc alkoxides and aryloxides supported by commercially available ligands as promoters of chemical transformations of lactic acid derivatives to industrially important fine chemicals
    Authors:
    Rafał Petrus, Piotr Sobota
    Academic press:
    Coordination Chemistry Reviews (rok: 2019, tom: 396, strony: 72-88), Wydawca: ELSEVIER
    Status:
    Published
    DOI:
    10.1016/j.ccr.2019.06.002 - link to the publication
  4. Solvothermal Alcoholysis Method for Recycling High-Consistency Silicone Rubber Waste
    Authors:
    Rafał Petrus*, Józef Utko, Radosław Gniłka, Mariusz G. Fleszar, Tadeusz Lis, and Piotr Sobota*
    Academic press:
    Macromolecules (rok: 2021, tom: 54, strony: 2449–2465), Wydawca: ACS
    Status:
    Published
    DOI:
    10.1021/acs.macromol.0c02773 - link to the publication
  5. Convenient Route to Heterometallic Group 4−Zinc Precursors for Binary Oxide Nanomaterials
    Authors:
    Rafał Petrus,Katarzyna Chomiak, Józef Utko, Magdalena Wilk-Kozubek, Tadeusz Lis, Joanna Cybińska, and Piotr Sobota
    Academic press:
    Inorganic Chemistry (rok: 2020, tom: 59, strony: 8108-8120), Wydawca: American Chemical Society
    Status:
    Published
    DOI:
    10.1021/acs.inorgchem.0c00399 - link to the publication
  6. Heterometallic Group 4−Lanthanide Oxo-alkoxide Precursors for Synthesis of Binary Oxide Nanomaterials
    Authors:
    Rafał Petrus,Katarzyna Chomiak, Józef Utko, Alina Bieńko, Tadeusz Lis, and Piotr Sobota
    Academic press:
    Inorganic Chemistry (rok: 2020, tom: 59, strony: 16545-16556), Wydawca: American Chemical Society
    Status:
    Published
    DOI:
    10.1021/acs.inorgchem.0c02478 - link to the publication
  7. Use of lithium aryloxides as promoters for preparation of α-hydroxy acid esters
    Authors:
    Rafał Petrus, Patryk Fałata and Piotr Sobota
    Academic press:
    Dalton Transactions (rok: 2020, tom: 49, strony: 866), Wydawca: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/c9dt03631h - link to the publication