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Development of high performance catalysts/reactors systems for cascade/tandem reactions. Case studies of application in dynamic kinetic resolution of racemates.

2016/23/B/ST8/00627

Keywords

Descriptors

  • ST8_1: Inżynieria chemiczna, chemia techniczna, inżynieria środowiska, inżynieria sanitarna, inżynieria procesowa

Panel

ST8 – Production and processes engineering: modelling, product design, process design and control, construction methods and engineering, power units and systems

Host institution

Politechnika Śląska, Wydział Chemiczny

Voivodeship: śląskie

Other projects carried out by the institution »

Principal investigator (from the host institution)

prof. Andrzej Bolesław Jarzębski

Number of co-investigators in the project: 8

Call

OPUS 12 – announced on 2016-09-15

Amount awarded
877 600 PLN
Project start date
2017-08-09
Project end date
2021-11-08
Project duration
51 months (the same as in the proposal)
Project status
Project settled

Project description

Download the project description in a pdf file

Note — project descriptions were prepared by the authors of the applications themselves and placed in the system in an unchanged form.

Equipment purchased [PL]

  1. Kolumny chromatograficzne (3 pcs). Cost: 30 000 PLN
  2. Mieszadło magnetyczne (2 pcs). Cost: 8 000 PLN
  3. Pompa. Cost: 11 000 PLN
  4. Spektrometr FTIR. Cost: 160 000 PLN
  5. Wyparka rotacyjna. Cost: 42 000 PLN

Information in the final report

Publication in academic press/journals (5)

  1. Continuous flow kinetic resolution of a non-equimolar mixture of diastereoisomeric alcohol using a structured monolithic enzymatic microreactor

    Authors:
    D. Strub, K. Szymańska, Z. Hrydziuszko, J. Bryjak, A. Jarzębski
    Academic press:
    Reaction Chemistry & Engineering (year: 2019, volume: -, pages: -), Publisher: RSC
    Status:
    Published
    DOI:
    10.1039/C8RE00177D – link to the publication

  2. Rotating bed reactor packed with heterofunctional structured silica-supported lipase. Developing an effective system for the organic solvent and aqueous phase reactions

    Authors:
    D. Kowalczykiewicz, K. Szymańska, D. Gillner, A.B. Jarzębski
    Academic press:
    Microporous and Mesoporous Materials (year: 2021, volume: 312, pages: 110789), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.micromeso.2020.110789 – link to the publication

  3. Lipase immobilized on MCFs as biocatalysts for kinetic and dynamic kinetic resolution of sec-alcohols

    Authors:
    D. Stradomska, M. Heba, A. Czernek, A N. Kuźnik, D. Gillner, K. Maresz, W. Pudło, A. Jarzębski, K. Szymańska
    Academic press:
    Catalysts (year: 2021, volume: 11(4), pages: 518), Publisher: MDPI
    Status:
    Published
    DOI:
    10.3390/catal11040518 – link to the publication

  4. Catalytic Functionalized Structured Monolithic Micro-/Mesoreactors: Engineering, Properties, and Performance in Flow Synthesis: An Overview and Guidelines

    Authors:
    K. Szymańska, A. Ciemięga, K. Maresz, W. Pudło, J. Malinowski, J. Mrowiec-Białoń, A. B. Jarzębski,
    Academic press:
    Frontiers in Chemical Engineering (year: 2021, volume: 3, pages: 789102), Publisher: Frontiers
    Status:
    Published
    DOI:
    10.3389/fceng.2021.789102 – link to the publication

  5. Engineering and performance of ruthenium complexes immobilized on mesoporous siliceous materials as racemization catalysts

    Authors:
    M. Heba, D. Stradomska, K. Szymańska, A. Jarzębski, K. Ambroziak, M. Masternak, A. Kolanowska, W. Pudło, N. Kuźnik
    Academic press:
    Catalysts (year: 2021, volume: 11, pages: 316), Publisher: MDPI
    Status:
    Published
    DOI:
    10.3390/catal11030316 – link to the publication

Articles in post-conference publications (20)

  1. Nanocząsteczki palladu osadzone na krzemionce-heterogeniczne katalizatory racemizacji amin

    Authors:
    S. Stradomska, K.Szymańska, A. Jarzębski
    Conference:
    Pomiędzy Naukami - VII Ogólnopolska Konferencja dla Młodych Naukowców (year: 2018, pages: 67), Publisher: Uniwersytet Śląski
    Date:
    conference 14.09.2018
    Status:
    Published

  2. Dynamiczny rozdział kinetyczny (rac)-fenyloetanolu

    Authors:
    D. Stradomska, M. Zaufał, K. Szymańska, N. Kuźnik, A. Jarzębski
    Conference:
    Nowe trendy w badaniach naukowych (year: 2021, pages: 30), Publisher: CREATIVETIME
    Date:
    conference 26-28.02.2021
    Status:
    Published

  3. Ultra fast synthesis of fine chemicals

    Authors:
    Katarzyna Szymańska, Julita Mrowiec-Białoń, Andrzej Jarzębski
    Conference:
    LI Ogólnopolskie Kolokwium Katalityczne (year: 2019, pages: 11), Publisher: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera PAN
    Date:
    conference 20-22.03.2019
    Status:
    Published

  4. Synteza biologicznie aktywnych pochodnych alfa-aminobisfosfonianów

    Authors:
    M. Zaufal, K. Juszczak, A. Kuźnik
    Conference:
    Dokonania naukowe doktorantów, edycja VII (year: 2019, pages: 115), Publisher: CREATIVETIME
    Date:
    conference 06.04.2019
    Status:
    Published

  5. Enzymatic chiral cyanohydrins synthesis in continuous flow microreactor

    Authors:
    D. Stradomska, J. Coloma, U. Hanefeld, K. Szymańska
    Conference:
    Symbioza (year: 2021, pages: 2021), Publisher: Faculty of Biology, University of Warsaw
    Date:
    conference 21-23.05.2021
    Status:
    Published

  6. Kinetic resolution of phenylethylamine using rotating bed reactor

    Authors:
    Dominika Stradomska, Katarzyna Szymańska, Andrzej Jarzebski
    Conference:
    8th edition of the conference for young scientists Science beyond disciplines (year: 2019, pages: 83), Publisher: Harit
    Date:
    conference 19-20.09.2019
    Status:
    Published

  7. Immobilizowane kompleksy rutenu na nosnikach krzemionkowych i węglowych

    Authors:
    M. Heba, D. Stradomska, N. Kuźnik
    Conference:
    e-Zjazd Wiosenny SSPTChem 2021 (year: 2021, pages: 83), Publisher: -
    Date:
    conference 27-29.05.2021
    Status:
    Published

  8. Kompleksy metali jako katalizatory racemizacji w dynamicznym rozdziale kinetycznym

    Authors:
    M. Zaufal, D. Stradomska, N. Kuźnik
    Conference:
    Dokonania naukowe doktorantów, edycja VII (year: 2019, pages: 117), Publisher: CREATIVETIME
    Date:
    conference 06.04.2019
    Status:
    Published

  9. Dynamic kinetic resolution of primary amines using rotating bed reactor

    Authors:
    Dominika Stradomska, Katarzyna Szymańska, Andrzej Jarzębski
    Conference:
    8th Intercollegiate Biotechnology Symposium Symbioza (year: 2019, pages: 156), Publisher: Wydział Biologi UW
    Date:
    conference 17-19. 05.2019
    Status:
    Published

  10. Continuous flow kinetic resolution of diastereoisomeric alcohol using structures monolithic enzymatic microreactor

    Authors:
    D. Strub, K. Szymańska, Z. Hrydziuszko, J. Bryjak, A. Jarzębski
    Conference:
    23rd Polish conference of Chemical and Process Engineering (year: 2019, pages: 167), Publisher: Politechnika Warszawska
    Date:
    conference 2-5.06.2019
    Status:
    Published

  11. Nanocząstki palladu osadzone na monolitach krzeminkowych jako katalizatory racemizacji amin

    Authors:
    D. Stradomska, K. Szymańska, A. Jarzebski
    Conference:
    VII Łódzkie Sympozjum Doktorantów Chemii (year: 2019, pages: 53), Publisher: Wydawnictwo Politechniki Łódzkiej
    Date:
    conference 9-10.05.2019
    Status:
    Published

  12. Nanostructured monolithic microreactors for ultra fast synthesis of fine chemicals

    Authors:
    K.Szymańska, J. Mrowiec-Białoń, A. Jarzębski
    Conference:
    23rd Polish conference of Chemical and Process Engineering (year: 2019, pages: 172), Publisher: Politechnika Warszawska
    Date:
    conference 2-5.06.2019
    Status:
    Published

  13. Zastosowanie enzymów w dynamicznym rozdziale kinetycznym

    Authors:
    M. Heba, D. Stradomska, N. Kuźnik
    Conference:
    Enzymos (year: 2021, pages: 55), Publisher: Tygiel
    Date:
    conference 05.02.2021
    Status:
    Published

  14. Dynamiczny rozdział kinetyczny (rac)-fenyloetanolu

    Authors:
    D. Stradomska, M. Zaufal, K. Szymańska, N. Kuźnik, A. Jarzębski
    Conference:
    Nowe trendy w badaniach naukowych (year: 2021, pages: 30), Publisher: Creativetime
    Date:
    conference 26-28.02.2021
    Status:
    Published

  15. Zastosowanie enzymów w dynamicznym rozdziale kinetycznym

    Authors:
    M. Heba, D. Stradomska, N. Kuźnik
    Conference:
    V Konferencja naukowa ENZYMOS, Enzymy w nauce i przemyśle (year: 2021, pages: 55-56), Publisher: TYGIEL
    Date:
    conference 05.02.2021
    Status:
    Published

  16. Hierarchically structured continuous monolithic microreactors: application potential in biotransformations

    Authors:
    K. Szymańska, A.Jarzębski
    Conference:
    The 4th Symposium on Biotransformations for Pharmaceutical and Cosmetic Industry (year: 2018, pages: 37), Publisher: Uniwersytet Wrocławski
    Date:
    conference 25-27. 06.2018
    Status:
    Published

  17. Immobilizowane kompleksy rutenu jako heterogeniczne katalizatory racemizacji

    Authors:
    M.Heba, D. Stradomska, N. Kuźnik
    Conference:
    XIII Interdyscyplinarna Konferencja Naukowa TYGIEL 2021 Interdyscyplinarność Kluczem rozwoju (year: 2021, pages: 182-183), Publisher: TYGIEL
    Date:
    conference 25-28.03.2021
    Status:
    Published

  18. Chelatujące ligandy azotowo-tlenowe, a ich szerokie zastosowanie

    Authors:
    M. Zaufal, K. Bakalorz, A. Kuźnik, S. Skubisz, N. Kuźnik
    Conference:
    Dokonania naukowe doktorantów, edycja VII (year: 2019, pages: 116), Publisher: CREATIVETIME
    Date:
    conference 06.04.2019
    Status:
    Published

  19. The catalytic dynamic kinetic resolution of secondary alcohols

    Authors:
    D. Bochenek, M.Zaufal, N. Kuźnik, D. Gillner, A. Jarzębski
    Conference:
    The 4th Symposium on Biotransformations for Pharmaceutical and Cosmetic Industry (year: 2018, pages: 45), Publisher: Uniwersytet Wrocławski
    Date:
    conference 25-27.06.2018
    Status:
    Published

  20. Chemical and enzymatic methods for the synthesis of levulinic acid esters

    Authors:
    D. Gillner, M. Przypis, D. Kowalczykiewicz, P.Wójcik, K. Matuszek, A. Chrobok, K. Szymańska, A. Jarzębski
    Conference:
    The 4th Symposium on Biotransformations for Pharmaceutical and Cosmetic Industry (year: 2018, pages: 23), Publisher: Uniwersytet Wrocławski
    Date:
    conference 25-27.06.2018
    Status:
    Published

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Graphic design and implementation: Jakub Piotrowski