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New platinum and rhodium complexes with bulky N-heterocyclic carbene ligands - synthesis, structure and catalytic activity.

2016/23/D/ST5/00417

Keywords

Descriptors

  • ST5_14: Chemia koordynacyjna
  • ST5_18: Kataliza homogeniczna i heterogeniczna
  • ST5_23: Chemia organiczna

Panel

ST5 – Materials: materials synthesis, structure-properties relations, advanced and functional materials with designed properties, (macro)molecular architecture, material engineering

Host institution

Uniwersytet im. Adama Mickiewicza w Poznaniu, Wydział Chemii

Voivodeship: wielkopolskie

Other projects carried out by the institution »

Principal investigator (from the host institution)

dr Patrycja Żak

Number of co-investigators in the project: 5

Call

SONATA 12 – announced on 2016-09-15

Amount awarded
520 000 PLN
Project start date
2017-07-12
Project end date
2021-07-11
Project duration
48 months (the same as in the proposal)
Project status
Project settled

Project description

Download the project description in a pdf file

Note — project descriptions were prepared by the authors of the applications themselves and placed in the system in an unchanged form.

Equipment purchased [PL]

  1. Chromatograf gazowy. Cost: 120 000 PLN
  2. Mieszadła magnetyczne z grzaniem i osprzętem (2 pcs). Cost: 7 000 PLN
  3. Rotacyjna pompa próżniowa. Cost: 11 000 PLN
  4. Zestaw komputerowy. Cost: 5 000 PLN

Information in the final report

Publication in academic press/journals (8)

  1. Highly efficient route for the synthesis of a novel generation of tetraorganofunctional double-decker type of silsesquioxanes

    Authors:
    J. Duszczak, K. Mituła, R. Januszewski, P. Żak, B. Dudziec, B. Marciniec
    Academic press:
    ChemCatChem (year: 2019, volume: 11, pages: 1086-1091), Publisher: ChemPubSoc
    Status:
    Published
    DOI:
    10.1002/cctc.201801609 – link to the publication

  2. Polysiloxanes Grafted with Mono(alkenyl)Silsesquioxanes-Particular Concept for their Connection

    Authors:
    Katarzyna Mituła, Julia Duszczak, M. Rzonsowska, Patrycja Żak, Beata Dudziec
    Academic press:
    Materials (year: 2020, volume: 13, pages: 4784 1-16), Publisher: MDPI
    Status:
    Published
    DOI:
    10.3390/ma13214784 – link to the publication

  3. Selective synthesis of E-vinylsilanes and E,E-divinylsilanes via platinum-catalyzed hydrosilylation of alkynes with secondary silanes

    Authors:
    P. Żak, M. Bołt, C. Pietraszuk
    Academic press:
    RSC Advances (year: 2018, volume: 8, pages: 40016-40021), Publisher: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/C8RA08640K – link to the publication

  4. Highly selective hydrosilylation of olefins and acetylenes by platinum(0) complexes bearing bulky N-heterocyclic carbene ligands

    Authors:
    P. Żak, M. Bołt, M. Kubicki, C. Pietraszuk
    Academic press:
    Dalton Transactions (year: 2018, volume: 47, pages: 1903-1910), Publisher: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/c7dt04392a – link to the publication

  5. Selective hydrosilylation of dienes, enynes and diynes catalyzed by platinum complex with very bulky NHC ligand – crucial role of precise tuning of the reaction conditions,

    Authors:
    P. Żak, M. Bołt, C. Pietraszuk
    Academic press:
    European Journal Of Inorganic Chemistry (year: 2019, volume: -, pages: 2455–2461), Publisher: ChemPubSoc
    Status:
    Published
    DOI:
    10.1002/ejic.201900217 – link to the publication

  6. Synthesis of (E)-1,4-disilsesquioxylsubstitiuted but-1-en-3-ynes via platinum-catalyzed dimerization of ethynylsiloxysilsesquioxanes

    Authors:
    P. Żak, M. Bołt, B. Dudziec, M. Kubicki
    Academic press:
    Dalton Transactions (year: 2019, volume: 48, pages: 2657-2663), Publisher: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/c8dt05142a – link to the publication

  7. Kompleksy platyny typu Markó zawierające N-heterocykliczne ligandy karbenowe o właściwościach supersterycznych, Wiadomości Chemiczne

    Authors:
    Małgorzata Bołt, Patrycja, Żak
    Academic press:
    Wiadomości Chemiczne (year: 2020, volume: 75, pages: 31-52), Publisher: PTChem
    Status:
    Published

  8. Application of bulky NHC-rhodium complexes in efficient S-Si and S-S bonds forming reactions

    Authors:
    Małgorzata Bołt, Patrycja Żak
    Status:
    Accepted for publication

Articles in post-conference publications (6)

  1. Katalizowana kompleksami platyny regio- i stereoselektywna metoda syntezy związków krzemoorganicznych

    Authors:
    P. Żak, M Bołt, C. Pietraszuk
    Conference:
    61 Zjazd Naukowy Polskiego Towarzystwa Chemicznego (year: 2018, pages: S03-8), Publisher: PTChem
    Date:
    conference 17-21.09.2018
    Status:
    Published

  2. Wysoce selektywne hydrosililowanie olefin i acetylenów katalizowane kompleksami platyny(0) z N-heterocyklicznymi ligandami karbenowymi o właściwościach supersterycznych

    Authors:
    M. Bołt, P. Żak, J. Lorkowski.M. Kubicki, C. Pietraszuk
    Conference:
    IV Poznańskie Sympozjum Młodych Naukowców (year: 2017, pages: PS19 str 90), Publisher: -
    Date:
    conference 18.11.2017
    Status:
    Published

  3. Controlling the regio- and stereoselectivity of hydrosilylation reaction catalyzed by platinum (0) complexes bearing bulky NHC ligand

    Authors:
    M. Bołt, P. Żak, C. Pietraszuk
    Conference:
    10th European Organic Chemistry Congress (year: 2019, pages: 60), Publisher: Organic Chemistry: Current Research
    Date:
    conference 2019-03-21-22
    Status:
    Published

  4. Katalizowana kompleksami platyny regio- i stereoselektywna metoda syntezy związków krzemo organicznych

    Authors:
    P. Żak, M. Bołt, C. Pietraszuk
    Conference:
    61. Zjazd Naukowy Polskiego Towarzystwa Chemicznego (year: 2019, pages: S03-8), Publisher: PTChem
    Date:
    conference 2019-09-17-21
    Status:
    Published

  5. Katalizowane N-heterocyklicznymi kompleksami rodu efektywne metody tworzenia wiązań S-S, S-Si i S-C

    Authors:
    Patrycja Żak, Małgorzata Bołt
    Conference:
    63. Zjazd Naukowy Polskiego Towarzystwa Chemicznego (year: 2021, pages: SO1 KS13 str 106), Publisher: Polskie Towarzystwo Chemiczne
    Date:
    conference 13-14.09.2021
    Status:
    Published

  6. Controlling the regio- and stereoselectivity of hydrosilylation reaction catalyzed by platinum (0) complexes bearing bulky NHC ligand

    Authors:
    M. Bołt, P. Żak, C. Pietraszuk
    Conference:
    5th Edition of Global Conference on Catalysis, Chemical Engineering and Technology (year: 2019, pages: 103), Publisher: -
    Date:
    conference 2019-09-16-18
    Status:
    Published

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Graphic design and implementation: Jakub Piotrowski