Projects funded by the NCN

Information on the principal investigator and host institution

Information of the project and the call

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An elaboration of analytical method for detection of non-steroidal anti-inflammatory drugs in equestrian nutritional and dietary supplements and investigation of these preparations for the presence of doping agents

2016/21/N/ST4/02342

Keywords:

doping agents non-steroidal anti-inflammatory drugs NSAIDs anabolic-androgenic steroids AAS stimulants equestrian dietary and nutritional supplements, GC-MS

Descriptors:

  • ST4_6: Instrumental methods in chemistry
  • ST4_3: Molecular architecture and structure

Panel:

ST4 - Chemistry: physical chemistry/chemical physics, theoretical chemistry, analytical chemistry, inorganic chemistry, organic chemistry, method development

Host institution :

Instytut Sportu - Państwowy Instytut Badawczy

woj. mazowieckie

Other projects carried out by the institution 

Principal investigator (from the host institution):

Emilia Waraksa 

Number of co-investigators in the project: 3

Call: PRELUDIUM 11 - announced on 2016-03-15

Amount awarded: 99 040 PLN

Project start date (Y-m-d): 2017-04-03

Project end date (Y-m-d): 2019-04-02

Project duration:: 24 months (the same as in the proposal)

Project status: Project settled

Project description

Download the project description in a pdf file

Note - project descriptions were prepared by the authors of the applications themselves and placed in the system in an unchanged form.

Equipment purchased [PL]

  1. Koncentrator blokowy (27 995 PLN)

Information in the final report

  • Publication in academic press/journals (7)
  • Articles in post-conference publications (2)
  1. Determination of bromhexine and its metabolites in equine serum samples by liquid chromatography – tandem mass spectrometry: Applicability to the elimination study after single oral dose
    Authors:
    E. Waraksa, K. Owczarek, P. Kubica, E. Kłodzińska, M. Ozimek, R. Wrzesień, B. Bobrowska-Korczak, J. Namieśnik
    Academic press:
    Journal of Chromatography B (rok: 2020, tom: 1151, strony: 122197), Wydawca: Springer
    Status:
    Published
    DOI:
    10.1016/j.jchromb.2020.122197 - link to the publication
  2. Nonsteroidal anti-inflammatory drug metabolism studies in horses in view of doping control: Analytical strategies and challenges
    Authors:
    E. Waraksa, W. Filipiak, E. Kłodzińska, M. Ozimek, M. Konop, J. Namieśnik
    Academic press:
    Analytical Methods (rok: 2019, tom: 11, strony: 3767), Wydawca: Royal Society of Ciemistry
    Status:
    Published
    DOI:
    10.1039/c9ay00692c - link to the publication
  3. Determination of free tyrosine in equestrian supplements by LC–MS/MS and comparison of its quantity with total free amino acids content in view of doping control
    Authors:
    E. Waraksa, K. Kowalski, R. Rola, E. Kłodzińska, T. Bieńkowski, J. Namieśnik
    Academic press:
    Microchemical Journal (rok: 2019, tom: 146, strony: 56-65), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.microc.2018.12.033 - link to the publication
  4. A rapid and sensitive method for quantitative analysis of ibuprofen and its metabolites in equine urine samples by gas chromatography-tandem mass spectrometry
    Authors:
    E. Waraksa, M.K. Woźniak, E. Kłodzińska, R. Wrzesień, B. Bobrowska-Korczak, J. Namieśnik
    Academic press:
    Journal of Separation Science (rok: 2018, tom: 41, strony: 3881), Wydawca: Wiley Online Library
    Status:
    Published
    DOI:
    10.1002/jssc.201800614 - link to the publication
  5. Quantification of unconjugated and total ibuprofen and its metabolites in equine urine samples by gas chromatography–tandem mass spectrometry: Application to the excretion study
    Authors:
    E. Waraksa, M.K. Woźniak, L. Banaszkiewicz, E. Kłodzińska, M. Ozimek, R. Wrzesień, B. Bobrowska-Korczak, J. Namieśnik
    Academic press:
    Microchemical Journal (rok: 2019, tom: 150, strony: 104129), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.microc.2019.104129 - link to the publication
  6. A rapid and eco-friendly method for determination of the main components of gamma-oryzanol in equestrian dietary and nutritional supplements by liquid chromatography—tandem mass spectrometry
    Authors:
    E. Waraksa, K. Kowalski, E. Kłodzińska, R. Rola, J. Ciekot, W. Filipiak, T. Bieńkowski, J. Namieśnik
    Academic press:
    Journal of Pharmaceutical and Biomedical Analysis (rok: 2019, tom: 172, strony: 339-348), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.jpba.2019.04.029 - link to the publication
  7. Comparison of GC–MS and MEKC methods for caffeine determination in preworkout supplements
    Authors:
    E. Waraksa, A. Pokrywka, M. Konop, J. Namieśnik, E. Kłodzińska
    Academic press:
    Electrophoresis (rok: 2019, tom: 40, strony: 1540), Wydawca: Wiley Online Library
    Status:
    Published
    DOI:
    10.1002/elps.201800512 - link to the publication
  1. Oznaczanie głównych składników gamma-oryzanolu i tyrozyny w odżywkach i suplementach diety z zastosowaniem chromatografii cieczowej sprzężonej z tandemową spektrometrią mas
    Authors:
    E. Waraksa, E. Kłodzińska, J. Namieśnik
    Conference:
    Międzynarodowy Zjazd Naukowego Polskiego Towarzystwa Medycyny Sportowej. Medycyna dla sportu, sport dla medycyny (rok: 2018, ), Wydawca: Medycyna Sportowa Polish Journal of Sports Medicine
    Data:
    konferencja 27-29.09.2018
    Status:
    Published
  2. Identyfikacja głównych składników gamma-oryzanolu w suplementach przeznaczonych dla koni
    Authors:
    E. Waraksa, E. Kłodzińska, J. Namieśnik
    Conference:
    III Konferencja Młodych Chemików Sądowych (rok: 2018, ), Wydawca: Wydział Chemii Uniwersytet Jagielloński w Krakowie
    Data:
    konferencja 15-16.04.2018 r.
    Status:
    Published

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