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Nanostructured semiconductor oxides - synthezis, modifications and characterization

2014/13/D/ST5/02750

Keywords

Descriptors

  • ST5_10: Nanomateriały: nanocząstki, nanorurki
  • ST5_6: Materiały porowate
  • ST4_9: Elektrochemia, elektrodializa, chemia w mikrostrumieniach

Panel

ST5 – Materials: materials synthesis, structure-properties relations, advanced and functional materials with designed properties, (macro)molecular architecture, material engineering

Host institution

Uniwersytet Jagielloński, Wydział Chemii

Voivodeship: małopolskie

Other projects carried out by the institution »

Principal investigator (from the host institution)

dr Leszek Zaraska

Number of co-investigators in the project: 3

Call

SONATA 7 – announced on 2014-03-17

Amount awarded
635 900 PLN
Project start date
2015-02-04
Project end date
2018-02-03
Project duration
36 months (the same as in the proposal)
Project status
Project settled

Equipment purchased [PL]

  1. Komputer przenośny wraz z drukarką.. Cost: 3 500 PLN
  2. Kriostat. Cost: 18 000 PLN
  3. Mieszadło magnetyczne (5 pcs). Cost: 5 000 PLN
  4. Moduł IPCE do spektrometru fotoelektrycznego. Cost: 26 260 PLN
  5. Multimiernik laboratoryjny o rozdzielczości odczytu 5 1/2 wraz z odpowiednim oprogramowaniem (2 pcs). Cost: 3 089 PLN
  6. Napylarka próżniowa do napylania metalami szlachetnymi oraz oksydującymi.. Cost: 130 000 PLN
  7. Programowalny zasilacz laboratoryjny niskich napięć (2 pcs). Cost: 6 000 PLN
  8. Programowalny zasilacz prądu stałego i zmiennego.. Cost: 63 439 PLN

Information in the final report

Publication in academic press/journals (7)

  1. Electrochemical growth of multisegment nanoporous tin oxide layers by applying periodically changed anodizing potential

    Authors:
    Leszek Zaraska, Karolina Gawlak, Dominika Gilek, Grzegorz D.Sulka
    Academic press:
    Applied Surface Science (year: 2018, volume: 455, pages: 1005-1009), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.apsusc.2018.06.044 – link to the publication

  2. Influence of anodizing conditions on generation of internal cracks in anodic porous tin oxide films grown in NaOH electrolyte

    Authors:
    Leszek Zaraska, Karolina Gawlak, Magdalena Gurgul, Magdalena Dziurka, Marlena Nowak, Dominika Gilek, Grzegorz D. Sulka
    Academic press:
    Applied Surface Science (year: 2018, volume: 439, pages: 672-680), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.apsusc.2017.12.188 – link to the publication

  3. Formation of crack-free nanoporous tin oxide layers via simple one-step anodic oxidation in NaOH at low applied voltages

    Authors:
    L. Zaraska, D. Gilek, K. Gawlak, M. Jaskuła, G.D. Sulka,
    Academic press:
    Applied Surface Science (year: 2016, volume: 390, pages: 31-37), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.apsusc.2016.08.043 – link to the publication

  4. Controlled synthesis of nanoporous tin oxide layers with various pore diameters and their photoelectrochemical properties

    Authors:
    Leszek Zaraska, Karolina Gawlak, Magdalena Gurgul, Damian K. Chlebda, Robert P. Socha, Grzegorz D. Sulka
    Academic press:
    Electrochimica Acta (year: 2017, volume: 254, pages: 238-245), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.electacta.2017.09.113 – link to the publication

  5. High aspect-ratio semiconducting ZnO nanowires formed by anodic oxidation of Zn foil and thermal treatment

    Authors:
    Leszek Zaraska, Krystyna Mika, Katarzyna E. Hnida, Marta Gajewska, Tomasz Łojewski, Marian Jaskuła, Grzegorz D. Sulka
    Academic press:
    Materials Science and Engineering B (year: 2017, volume: 226, pages: 94-98), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.mseb.2017.09.003 – link to the publication

  6. Formation of ZnO nanowires during anodic oxidation of zinc in bicarbonate electrolytes

    Authors:
    Leszek Zaraska, Krystyna Mika, Karolina Syrek, Grzegorz D. Sulka
    Academic press:
    Journal of Electroanalytical Chemistry (year: 2017, volume: 801, pages: 511–520), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.jelechem.2017.08.035 – link to the publication

  7. Nanoporous tin oxides synthesized via electrochemical anodization in oxalic acid and their photoelectrochemical activity

    Authors:
    Leszek Zaraska, Karolina Syrek, Katarzyna Hnida, Michał Bobruk, Aleksandra Krzysik, Tomasz Łojewski, Marian Jaskuła, Grzegorz D. Sulka
    Academic press:
    Electrochimica Acta (year: 2016, volume: 205, pages: 273-280), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.electacta.2016.02.023 – link to the publication

Articles in post-conference publications (27)

  1. Photoelectrochemical activity of nanoporous anodic oxide layers grown on tin in alkaline electrolytes

    Authors:
    K. Gawlak, K. Syrek, L. Zaraska, G.D. Sulka
    Conference:
    8th International Conference on Nanomaterials – Research and Application, Nanocon2016 (year: 2016, pages: 81), Publisher: TANGER Ltd.
    Date:
    conference 19-21.10.2016
    Status:
    Published

  2. Comparative study on anodic growth of nanoporous oxide layers on aluminum and tin

    Authors:
    K. Gawlak, A. Brudzisz, L. Zaraska, G.D. Sulka
    Conference:
    Electrochemistry 2016: Innovative, interdisciplinary, essential. (year: 2016, pages: H025), Publisher: Gesellschaft Deutscher Chemiker
    Date:
    conference 16-18.09.2016
    Status:
    Published

  3. Anodowe utlenianie metali jako obiecująca metoda otrzymywania nanostrukturalnych tlenków półprzewodnikowych o różnych morfologiach

    Authors:
    L. Zaraska, K. Gawlak, K. Mika, G.D. Sulka
    Conference:
    VIII Krajowa Konferencja Nanotechnologii (year: 2017, pages: 94), Publisher: Uniwersytet Łódzki
    Date:
    conference 20-23 VI 2017
    Status:
    Published

  4. The effect of anodizing parameters on the formation of ZnO nanowires during anodic oxidation of zinc in bicarbonate electrolytes

    Authors:
    K. Mika, L. Zaraska, G.D. Sulka
    Conference:
    Anodize it ! Conference (year: 2017, pages: 53), Publisher: Crimat Toulouse
    Date:
    conference 11-13.07.2017
    Status:
    Published

  5. Anodic growth of ZnO nanowires in bicarbonate electrolytes

    Authors:
    L. Zaraska, K. Mika, G.D. Sulka
    Conference:
    Chemistry and Chemical Technology (year: 2016, pages: 87), Publisher: Lithiuanian Society of Chemistry
    Date:
    conference 28-29.04.2016
    Status:
    Published

  6. Wpływ warunków syntezy na własciwości elektrochemiczne anodowego tlenku cyny

    Authors:
    L. Zaraska, K. Gawlak, M. Gurgul, K. Syrek, G.D. Sulka
    Conference:
    VIII Krajowa Konferencja Nanotechnologii (year: 2017, pages: 169), Publisher: Uniwersytet Łódzki
    Date:
    conference 20-23 VI 2017
    Status:
    Published

  7. Optymalizacja syntezy nanodrutów ZnO metodą anodowego utleniania w roztworach wodorowęglanów

    Authors:
    K. Mika, L. Zaraska, G.D. Sulka
    Conference:
    VIII Krajowa Konferencja Nanotechnologii (year: 2017, pages: 174), Publisher: Uniwersytet Łódzki
    Date:
    conference 20-23 VI 2017
    Status:
    Published

  8. Characterization of anodic oxide layers grown on tin in alkaline electrolyte

    Authors:
    K. Gawlak, M. Dziurka, K. Syrek, L. Zaraska, G.D. Sulka
    Conference:
    Electrochemistry 2016: Innovative, interdisciplinary, essential. (year: 2016, pages: L003), Publisher: Gesellschaft Deutscher Chemiker
    Date:
    conference 16-18.09.2016
    Status:
    Published

  9. Electrochemical synthesis of ZnO nanowire arrays

    Authors:
    K. Mika, L. Zaraska, G.D. Sulka
    Conference:
    International Workshop on Functional Nanoporous Materials FuNaM (year: 2016, pages: 64), Publisher: Uniwersytet Jagielloński, Wydział Chemii
    Date:
    conference 13-14.10.2016
    Status:
    Published

  10. Formation of multilayered nanoporous tin oxide films via potential-controlled anodization in NaOH

    Authors:
    D. Gilek, L. Zaraska, K. Gawlak, G.D. Sulka
    Conference:
    International Workshop on Functional Nanoporous Materials FuNaM (year: 2016, pages: 63), Publisher: Uniwersytet Jagielloński, Wydział Chemii
    Date:
    conference 13-14.10.2016
    Status:
    Published

  11. Formation of crack-free nanoporous tin oxide layers by simple anodization in alkaline electrolyte at low potentials

    Authors:
    L. Zaraska, D. Gilek, K. Gawlak, M. Jaskuła, G.D. Sulka
    Conference:
    Chemistry and Chemical Technology (year: 2016, pages: 86), Publisher: Lithiuanian Society of Chemistry
    Date:
    conference 28-29.04.2016
    Status:
    Published

  12. Nanostructured SnO2 layers with complex internal structure formed by anodic oxidation in alkaline electrolytes

    Authors:
    D. Gilek, L. Zaraska, K. Gawlak, M. Jaskuła, G.D. Sulka
    Conference:
    8th International Conference on Nanomaterials – Research and Application, Nanocon2016 (year: 2016, pages: 81-82), Publisher: TANGER Ltd.
    Date:
    conference 19-21.10.2016
    Status:
    Published

  13. ZnO nanowire arrays grown by simple anodic oxidation of Zn in bicarbonate electrolytes

    Authors:
    L. Zaraska, K. Mika, K. Syrek, G.D. Sulka,
    Conference:
    67th Annual Meeting of the International Society of Electrochemistry. Electrochemistry: from Sense to Sustainability, (year: 2016, pages: ise162342), Publisher: International Society of Electrochemistry
    Date:
    conference 21-26.10.2016
    Status:
    Published

  14. Anodic formation of crack-free multilayered nanoporous tin oxides

    Authors:
    L. Zaraska, D. Gilek, K. Gawlak, M. Jaskuła, G.D. Sulka,
    Conference:
    67th Annual Meeting of the International Society of Electrochemistry. Electrochemistry: from Sense to Sustainability (year: 2016, pages: ise162343), Publisher: International Society of Electrochemistry
    Date:
    conference 21-26.10.2016
    Status:
    Published

  15. Electrochemical growth of nanostructured tin oxide films

    Authors:
    L. Zaraska, M. Bobruk, A. Krzysik, M. Jaskuła, G.D. Sulka
    Conference:
    4th International Symposium on Surface Imaging/Spectroscopy at the Solid/Liquid Interface (year: 2015, pages: 57–58), Publisher: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera Polskiej Akademii Nauk
    Date:
    conference 2–4.09.2015
    Status:
    Published

  16. The effect of chemical and electrochemical polishing of tin on morphology of anodic tin oxide

    Authors:
    K.Gawlak, L.Zaraska, G.D.Sulka
    Conference:
    Chemistry and Chemical Technology (year: 2016, pages: 66), Publisher: Lithiuanian Society of Chemistry
    Date:
    conference 28-29.04.2016
    Status:
    Published

  17. The effect of ethanol on the growth and morphology of nanoporous tin oxide layers formed by anodization in alkaline electrolyte

    Authors:
    M. Nowak, M. Gurgul, K. Gawlak, L. Zaraska
    Conference:
    International Workshop on Functional Nanoporous Materials FuNaM (year: 2016, pages: 62), Publisher: Uniwersytet Jagielloński, Wydział Chemii
    Date:
    conference 13-14.0.2016
    Status:
    Published

  18. Anodic oxidation of metals - a simple and cost effective method for fabrication of nanostructured materials

    Authors:
    L. Zaraska, A. Brzózka, J. Kapusta-Kołodziej, M. Jarosz, E. Kurowska-Tabor, K. Syrek, A. Brudzisz, E. Wierzbicka, A. Pawlik, A. Krzysik, K. Mączka, A. Święs, E. Stanek, M. Zych, D. Szeliga, M. Jaskuła and G.D. Sulka
    Conference:
    7th Polish Conference on Nanotechnology (year: 2015, pages: 104), Publisher: Centrum NanoBioMedyczne UAM
    Date:
    conference 24-27.06.2015
    Status:
    Published

  19. Synthesis of nanoporous tin oxide layers via anodic oxidation of metallic Sn in acidic and alkaline electrolytes

    Authors:
    L. Zaraska, K. Gawlak, D. Gilek, G. Sulka
    Conference:
    Anodize it ! Conference (year: 2017, pages: 12), Publisher: Crimat Toulouse
    Date:
    conference 11-13.07.2017
    Status:
    Published

  20. Electrochemical synthesis of ZnO nanowires

    Authors:
    K. Mika, L. Zaraska, G.D. Sulka
    Conference:
    8th International Conference on Nanomaterials – Research and Application, Nanocon2016 (year: 2016, pages: 104), Publisher: TANGER Ltd.
    Date:
    conference 19-21.10.2016
    Status:
    Published

  21. Nanoporous semiconducting oxide layers electrochemically formed on Sn in alkaline electrolytes

    Authors:
    M. Dziurka, K. Gawlak, K. Syrek, L. Zaraska, G.D. Sulka
    Conference:
    International Workshop on Functional Nanoporous Materials FuNaM (year: 2016, pages: 67), Publisher: Uniwersytet Jagielloński, Wydział Chemii
    Date:
    conference 13-14.10.2016
    Status:
    Published

  22. Elektrochemiczne otrzymywanie nanodrutów ZnO

    Authors:
    K. Mika, L. Zaraska
    Conference:
    Horyzonty Nauki 2016 Forum Prac Dyplomowych (year: 2016, pages: 23-24), Publisher: Uniwersytet Jagielloński
    Date:
    conference 17-18.05.2016
    Status:
    Published

  23. Photoelectrochemical properties of nanoporous anodic tin oxide layers

    Authors:
    K. Gawlak, L. Zaraska, M. Gurgul, K. Syrek, G. D. Sulka
    Conference:
    21st Topical Meeting of the International Society of Electrochemistry - Photoelectrochemistry of semiconductor at the nanoscale: from fundamental aspects to practical applications (year: 2017, pages: top170195), Publisher: International Society of Electrochemistry
    Date:
    conference 23–26 IV 2017
    Status:
    Published

  24. Anodic formation of ZnO nanostructures

    Authors:
    L. Zaraska, K. Mika, G.D. Sulka
    Conference:
    4th International Symposium on Surface Imaging/Spectroscopy at the Solid/Liquid Interface (year: 2015, pages: 174), Publisher: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera Polskiej Akademii Nauk
    Date:
    conference 2–4.09.2015
    Status:
    Published

  25. Nanoporous anodic SnO2 and its photoelectrochemical properties

    Authors:
    L. Zaraska, M. Bobruk, A. Krzysik, K. Syrek, G.D. Sulka
    Conference:
    21st International Symposium on the Photochemistry and Photophysics of Coordination Compounds (year: 2015, pages: 241), Publisher: Uniwersytet Jagielloński
    Date:
    conference 5-9.07.2015
    Status:
    Published

  26. Anodic oxidation as a simple and cost-effective method for fabrication of nanostructured semiconductor oxides with various morphologies

    Authors:
    L. Zaraska, K. Gawlak, K. Mika, K. Syrek, M. Zych, D. Gilek, G.D. Sulka
    Conference:
    21st Topical Meeting of the International Society of Electrochemistry - Photoelectrochemistry of semiconductor at the nanoscale: from fundamental aspects to practical applications (year: 2017, pages: top170210), Publisher: International Society of Electrochemistry
    Date:
    conference 23–26 IV 2017
    Status:
    Published

  27. Porous anodic tin oxides formed in various electrolytes

    Authors:
    L. Zaraska, A. Krzysik, D. Gilek, G.D. Sulka, M. Jaskuła
    Conference:
    4th International Symposium on Surface Imaging/Spectroscopy at the Solid/Liquid Interface (year: 2015, pages: 173), Publisher: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera Polskiej Akademii Nauk
    Date:
    conference 2–4.09.2015
    Status:
    Published

Book publications / chapters in book publications (1)

  1. Anodic growth of nanoporous tin oxide layers in acidic electrolytes

    Authors:
    L. Zaraska, K. Gawlak, A. Krzysik, M. Jaskuła,
    Book:
    Promising materials and processes in technical electrochemistry (year: 2016, volume: nie dotyczy, pages: 194-198), Publisher: Kyiv National University of Technologies and Design
    Status:
    Published

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Graphic design and implementation: Jakub Piotrowski