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The implementation of time-resolved Rapid Scan FT-IR spectroscopy for investigation of nature of active sites and transformation of reagent molecules in micro/mesoporous materials

2014/13/D/ST5/02761

Keywords

Descriptors

  • ST5_6: Materiały porowate
  • ST5_18: Kataliza homogeniczna i heterogeniczna
  • ST5_19: Metody badań właściwości materiałów

Panel

ST5 – Materials: materials synthesis, structure-properties relations, advanced and functional materials with designed properties, (macro)molecular architecture, material engineering

Host institution

Uniwersytet Jagielloński, Wydział Chemii

Voivodeship: małopolskie

Other projects carried out by the institution »

Principal investigator (from the host institution)

dr Karolina Anna Tarach

Number of co-investigators in the project: 7

Call

SONATA 7 – announced on 2014-03-17

Amount awarded
667 980 PLN
Project start date
2015-02-04
Project end date
2018-06-03
Project duration
40 months (the same as in the proposal)
Project status
Project settled

Equipment purchased [PL]

  1. Czasowo-rozdzielczy spektrometr Rapid Scan FT-IR z akcesoriami. Cost: 300 000 PLN
  2. Elementy wyposażenia komory reakcyjnej IR. Cost: 11 697 PLN
  3. Komputer. Cost: 4 000 PLN
  4. Pompa próżniowa. Cost: 16 000 PLN

Information in the final report

Publication in academic press/journals (7)

  1. Quantitative infrared spectroscopic studies and 2D COS analysis of xylenes isomerization over hierarchical zeolites

    Authors:
    Karolina A. Tarach, Kinga Gołąbek, Minkee Choi, Kinga Góra-Marek
    Academic press:
    Catalysis Today (year: 2017, volume: 283, pages: 158-171), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.cattod.2016.02.035 – link to the publication

  2. Alkaline-acid treated zeolite L as catalyst in ethanol dehydration process

    Authors:
    Karolina A. Tarach, Justyna Tekla, Urszula Filek, Agnieszka Szymocha, Iwona Tarach, Kinga Góra-Marek
    Academic press:
    Microporous and Mesoporous Materials (year: 2017, volume: 241, pages: 132-144), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.micromeso.2016.12.035 – link to the publication

  3. Modification of ferrierite through post-synthesis treatments. Acidic and catalytic properties

    Authors:
    Kamila Brylewska, Karolina A. Tarach, Włodzimierz Mozgawa, Zbigniew Olejniczak, Urszula Filek, Kinga Góra-Marek
    Academic press:
    Journal of Molecular Structure (year: 2016, volume: 1126, pages: 147-153), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.molstruc.2015.12.046 – link to the publication

  4. Acidity and accessibility studies of desilicated ZSM-5 zeolites in terms of their effectiveness as catalysts in acid-catalyzed cracking processes

    Authors:
    Karolina A. Tarach, Kinga Góra-Marek Joaquin Martinez-Triguero, Ignacio Melián-Cabrera
    Academic press:
    Catalysis Science & Technology (year: 2017, volume: 7, pages: 858-873), Publisher: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/c6cy02609e – link to the publication

  5. Standard and rapid scan infrared spectroscopic studies of o-xylene transformations in terms of pore arrangement of 10-ring zeolites – 2D COS analysis

    Authors:
    Kinga Gołąbek, Karolina A. Tarach, Kinga Góra-Marek
    Academic press:
    Dalton Transactions (year: 2017, volume: 46, pages: 9934-9950), Publisher: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/c7dt00644f – link to the publication

  6. Ethylene formation by dehydration of ethanol over medium pore zeolites

    Authors:
    Kinga Gołąbek, Karolina A. Tarach, Urszula Filek, Kinga Góra-Marek
    Academic press:
    Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy (year: 2018, volume: 192, pages: 464-472), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.saa.2017.11.049 – link to the publication

  7. Nickel loaded zeolites FAU and MFI: characterization and the activity in water-phase hydrodehalogenation of TCE

    Authors:
    Karolina A. Tarach, Anna Śrębowata, Emil Kowalewski, Kinga Gołąbek, Aldona Kostuch, Krzysztof Kruczała, Vladimir Girman, Kinga Góra-Marek
    Academic press:
    Applied Catalysis A: General (year: 2018, volume: 568, pages: 64-75), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.apcata.2018.09.026 – link to the publication

Articles in post-conference publications (19)

  1. The role of pore arrangement of 10-MR zeolites in transformation ethanol 2D COS analysis

    Authors:
    Kinga Gołąbek, Karolina A. Tarach, Urszula Filek, Kinga Góra-Marek
    Conference:
    EuropaCat (year: 2017, pages: 376-377), Publisher: European Research Institute of Catalysis
    Date:
    conference 27-31 sierpnia
    Status:
    Published

  2. IR studies of the interaction of organic molecules with acidic active sites in erionite

    Authors:
    Justyna Tekla, Karolina A. Tarach, Katarzyna Kwaśnik, Kinga Góra-Marek
    Conference:
    XIVth International Conference on Molecular Spectroscopy (year: 2017, pages: 59), Publisher: AGH University of Science and Technology
    Date:
    conference 3-7 września
    Status:
    Published

  3. Hierarchical erionites Preparation, physico-chemical properties and catalytic performances

    Authors:
    J. Tekla, K.A. Tarach, J.P. Gilson, L. Lakiss, K. Góra-Marek
    Conference:
    EuropaCat (year: 2017, pages: 485-486), Publisher: European Research Institute of Catalysis
    Date:
    conference 27-31 sierpnia
    Status:
    Published

  4. Application of 2D COS analysis for evaluation of xylene isomerization over 10-MR zeolites of various pore arrangement

    Authors:
    Karolina A. Tarach, Kinga Gołąbek, Kinga Góra-Marek
    Conference:
    EuropaCat (year: 2017, pages: 127-128), Publisher: European Research Institute of Catalysis
    Date:
    conference 27-31 sierpnia
    Status:
    Published

  5. IR Spectroscopic Studies of Xylenes Transformations - 2D COS Analysis

    Authors:
    Kinga Gołąbek, Karolina A. Tarach, Kinga Góra-Marek
    Conference:
    SpectroCat Workshop: Quantitative In-situ & Operando vibrational spectroscopies for Catalysis and Adsorption: state of the art, current limits and challenges (year: 2017, pages: 3), Publisher: SpectroCat Workshop Committee
    Date:
    conference 30-31 marca
    Status:
    Published

  6. Ethanol transformation over 10 MR zeolites – the role of pore architecture

    Authors:
    K.A. Tarach, K. Gołąbek, U. Filek, K. Góra-Marek
    Conference:
    FuNaM International Workshop on Functional Nanoporous Materials (year: 2016, pages: 28), Publisher: Marian Smoluchowski Consortium (KNOW)
    Date:
    conference 13-14 paźddziernika
    Status:
    Published

  7. Application of 2D COS analysis for evaluation of hydrocarbons isomerization over zeolites

    Authors:
    K.A. Tarach, K. Gołąbek, K. Góra-Marek
    Conference:
    XLVIII Ogólnopolskie Kolokwium Katalityczne (year: 2016, pages: 349-350), Publisher: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera PAN
    Date:
    conference 16-18 marca
    Status:
    Published

  8. Catalytic activity of hierarchical L zeolite in ethanol dehydration process

    Authors:
    Justyna Tekla, Karolina A. Tarach, Urszula Filek, Agnieszka Szymocha, Iwona Tarach, Kinga-Góra-Marek
    Conference:
    FuNaM International Workshop on Functional Nanoporous Materials (year: 2016, pages: 26), Publisher: Marian Smoluchowski Consortium (KNOW)
    Date:
    conference 13-14 paźddziernika
    Status:
    Published

  9. Application of nickel loaded zeolites in trichloroethylene removal from drinking water

    Authors:
    K.A. Tarach, A. Śrębowata, E. Kowalewski, K. Góra-Marek
    Conference:
    International Conference on Green Chemistry and Sustainable Engineering (year: 2016, pages: 49-50), Publisher: ScienceKNOW Conferences C.B.
    Date:
    conference 20-22 lipca
    Status:
    Published

  10. IR spectroscopic quantitative evaluation of substituted benzenes transformations over zeolites with well-adjusted mesopore system

    Authors:
    K. A. Tarach, J. Tekla, K.Góra-Marek
    Conference:
    5th International Conference on Operando Spectroscopy (year: 2015, pages: P 86), Publisher: International Operando Committee
    Date:
    conference 17-21 maja
    Status:
    Published

  11. Quantitative infrared spectroscopic evaluation of o-xylene isomerization over zeolites with well-adjusted mesopore system

    Authors:
    Karolina A. Tarach, Kinga Góra-Marek
    Conference:
    XX Zeolite Forum (year: 2015, pages: 129), Publisher: Polish Zeolite Association
    Date:
    conference 22-26 września
    Status:
    Published

  12. Nickel loaded zeolites in trichloroethylene removal from drinking water

    Authors:
    K. A. Tarach, E. Kowalewski, A. Śrębowata, K. Góra-Marek
    Conference:
    XLVIII Ogólnopolskie Kolokwium Katalityczne (year: 2016, pages: 310), Publisher: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera PAN
    Date:
    conference 16-18 marca
    Status:
    Published

  13. Ethanol transformation over 10 MR zeolites: the role of pore architecture

    Authors:
    K.A. Tarach, K. Gołąbek, U. Filek, K. Góra-Marek
    Conference:
    XLVIII Ogólnopolskie Kolokwium Katalityczne (year: 2016, pages: 167-168), Publisher: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera PAN
    Date:
    conference 16-18 marca
    Status:
    Published

  14. Ethanol transformation over 10 MR zeolites – the role of pore architecture

    Authors:
    K. Gołąbek , K.A. Tarach , U. Filek, K. Góra–Marek
    Conference:
    International Conference on Green Chemistry and Sustainable Engineering (year: 2016, pages: 53-54), Publisher: ScienceKNOW Conferences C.B.
    Date:
    conference 20-22 lipca
    Status:
    Published

  15. Microporous and hierarchical zeolites as catalysts of polyethylene cracking: role of acidity and porosity

    Authors:
    Karolina A. Tarach, I. Melian Cabrera, J. Martinez-Triguero, J. Datka, K. Góra-Marek
    Conference:
    XLVIII Ogólnopolskie Kolokwium Katalityczne (year: 2016, pages: 15-16), Publisher: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera PAN
    Date:
    conference 16-18 marca
    Status:
    Published

  16. Hierarchiczny zeolit L jako katalizator procesu dehydratacji etanolu

    Authors:
    J. Tekla, K.A Tarach, U. Filek, I. Tarach, K. Góra-Marek
    Conference:
    59 Zjazd Naukowy Polskiego Towarzystwa Chemicznego (year: 2016, pages: 251), Publisher: Polskie Towarzystwo Chemiczne
    Date:
    conference 19-23 września
    Status:
    Published

  17. Transformacja cząsteczki etanolu na zeolitach o kanałach 10-członowych – wpływ aranżacji porów

    Authors:
    K. Gołąbek, K.A. Tarach, K. Góra-Marek
    Conference:
    59 Zjazd Naukowy Polskiego Towarzystwa Chemicznego (year: 2016, pages: 251), Publisher: Polskie Towarzystwo Chemiczne
    Date:
    conference 19-23 września
    Status:
    Published

  18. Dwuwymiarowa spektroskopia korelacyjna 2D COS jako narzędzie analizy procesu izomeryzacji ksylenów na zeolitach o różnej architekturze porów

    Authors:
    K. Gołąbek, K.A. Tarach, K. Góra-Marek
    Conference:
    59 Zjazd Naukowy Polskiego Towarzystwa Chemicznego (year: 2016, pages: 245), Publisher: Polskie Towarzystwo Chemiczne
    Date:
    conference 19-23 września
    Status:
    Published

  19. Zeolity MFI jako efektywne katalizatory do krakingu HDPE oraz LDPE

    Authors:
    Kinga Gołąbek, K.A. Tarach, I. Melian Cabrera, J. Martinez-Triguero, J. Datka, K. Góra-Marek
    Conference:
    Wpływ Młodych Naukowców na Osiągnięcia Polskiej Nauki (year: 2015, pages: 100), Publisher: CREATIVETIME
    Date:
    conference 5 grudnia
    Status:
    Published

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