Microstructural and kinetic characterization of the phenomena occurring at the solder/substrate interfaces of the Ti-6Al-4V alloys brazed with the use amorphous TiZrCuPd ribbons.

2013/11/B/ST8/04286

Keywords

Descriptors

  • ST8_8: Inżynieria materiałowa (biomateriały, metale, ceramika, polimery, kompozyty)

Panel

ST8 – Production and processes engineering: modelling, product design, process design and control, construction methods and engineering, power units and systems

Host institution

Instytut Metalurgii i Inżynierii Materiałowej im. Aleksandra Krupkowskiego PAN

Voivodeship: małopolskie

Other projects carried out by the institution »

Principal investigator (from the host institution)

dr Anna Sypień

Number of co-investigators in the project: 5

Call

OPUS 6 – announced on 2013-09-16

Amount awarded
686 070 PLN
Project start date
2014-07-15
Project end date
2017-12-14
Project duration
41 months (the same as in the proposal)
Project status
Project settled

Equipment purchased [PL]

  1. Nagrzewnica indukcyjna (10-30 kHz, 40kW). Cost: 55 000 PLN
  2. Regulator temperatury.
  3. Układ próżniowy do lutowania w atmosferze ochronnej. Cost: 145 000 PLN

Information in the final report

Publication in academic press/journals (3)

  1. Modification of the Ti40Cu36Zr10Pd14 BMG Crystallization Mechanism with Heating Rates 10-140 K/min

    Authors:
    T. Czeppe, A. Sypien, and A. Wierzbicka-Miernik
    Academic press:
    Journal of Materials Engineering and Performance (year: 2016, volume: 25, pages: 5289-5301), Publisher: Springer
    Status:
    Published
    DOI:
    10.1007/s11665-016-2368-x – link to the publication
  2. Effect of Pd, temperature and time on wetting and interfacial microstructure of bulk metallic glasses TiCuZrPd on Ti-6Al-4V substrate.

    Authors:
    Anna Sypien, Kamil Badura, Przemyslaw Fima, Krzysztof Miernik
    Academic press:
    Journal of Alloys and Compounds (year: 2017, volume: 695, pages: 962-970), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.jallcom.2016.10.216 – link to the publication
  3. Thermomechanical behavior of amorphous alloys based on titanium at the temperature range of the glass transition and crystallization

    Authors:
    A. Sypien, G. Garzel, T. Czeppe
    Academic press:
    Materials Science & Engineering A (year: 2019, volume: 743, pages: 77-86), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.msea.2018.11.071 – link to the publication

Articles in post-conference publications (14)

  1. High-Temperature Oxidation Behavior of the TiCuZrPd Joint Produced by Vacuum Brazing

    Authors:
    Tomasz Czeppe, A. Sypien, Kamil Badura
    Conference:
    24th International Symposium on Metastable, Amorphous and Nanostructured Materials (year: 2017, pages: 92), Publisher: Arcady Zhukov
    Date:
    conference 18-23.06
    Status:
    Published
  2. Induction brazed Ti-6Al-4V alloy: Microstructure changes and phase transformation during annealing

    Authors:
    A.Sypien, Ł.Major, K. Badura and R. Chulist
    Conference:
    XVI International Conference ob Electron Microscopy EM2017 (year: 2017, pages: 155), Publisher: PTMI (Polish Society of Microscopy) and Faculty of materials Science and Engineering (Politechnika Warszawska)
    Date:
    conference 10-13.09.2017
    Status:
    Published
  3. Evaluation of microstructure and strength of induction brazed joints of TiAlV with Ti-based filler alloy

    Authors:
    A. Sypien
    Conference:
    13th International Conference on Diffusion in Solids and Liquids - DLS2017 (year: 2017, pages: 45-46), Publisher: DSL CONFERENCE
    Date:
    conference 26-30.06.2017
    Status:
    Published
  4. Brazing of Ti-6Al-4V alloy with new amorphous Ti-Zr-Cu-Pd-Sn filler foil

    Authors:
    Kamil badura, Anna Sypień
    Conference:
    13th Junior Euromat 2016 (year: 2016, pages: 26), Publisher: FEMS Federation of Europen Materials Societies
    Date:
    conference 10-14.07.2016
    Status:
    Published
  5. Microstructure characteristics of joints after induction brazing of Ti-6Al-4V alloy with Ti-Zr-Cu-Pd-Sn amorphous filler foil.

    Authors:
    K. Badura, A. Sypien
    Conference:
    EUROMAT2017 - European Congress and Exhibition on Advanced Materials and Processes (year: 2017, pages: 18), Publisher: Hellenic Metallurgical Society (HMS) and Hellenic Society for the Science & Technology of Condensed Matter (HSSTCM)
    Date:
    conference 17-22.09.2017
    Status:
    Published
  6. Wettability and interfacial microstructure characteristics of amorphous Zr52Ti24X14Cu10 (X=Ni, Pd) alloys on Ti-6Al-4V substrate

    Authors:
    K. Badura, A. Sypien, P. Fima
    Conference:
    XVI International Conference on Electron Microscopy, EM2017 (year: 2017, pages: 38), Publisher: PTMI (Polish Society of Microscopy) and Faculty of materials Science and Engineering (Politechnika Warszawska)
    Date:
    conference 1--13.09.2017
    Status:
    Published
  7. Induction heating technique applied for titanium brazing

    Authors:
    K. Badura, A. Sypien, W. Przybylo
    Conference:
    11th International Workshop on Subsecond Thermophysics (year: 2016, pages: 54), Publisher: Foundary Research Institute
    Date:
    conference 21-24.07.2016
    Status:
    Published
  8. Effect of brazing process parameters and the content of Pd on the growth of intermetallic phases in the joint TiAlV / TiCuZrPd / TiAlV

    Authors:
    A. Sypien, K. Badura, B. Kania
    Conference:
    EUROMAT2017 - European Congress and Exhibition on Advanced Materials and Processes (year: 2017, pages: 3), Publisher: Hellenic Metallurgical Society (HMS) and Hellenic Society for the Science & Technology of Condensed Matter (HSSTCM)
    Date:
    conference 17-22.09.2017
    Status:
    Published
  9. Crystallization of the Ti40Cu36Zr10Pd14 BMG studied with the high-rate DSC calorimetry

    Authors:
    T. Czeppe, A. Sypien, M. Stoica, A. Wierzbicka-Miernik and M. Szlezynger
    Conference:
    ISMANAM 2015 22-th International Symposium on Metastable Amorhous and Nanostructured Materials (year: 2015, pages: 129), Publisher: ISMANAM2015
    Date:
    conference 13-17.07
    Status:
    Published
  10. Influence of Pd addition on the wettability of amorphous TiCuZrPd alloys used as a filler during the brazing process.

    Authors:
    A.Sypien, P.Fima
    Conference:
    TMS2015 - 144 Annual Meeting and Exibiton 2015 (year: 2015, pages: 4), Publisher: WILEY
    Date:
    conference 15-19.03
    Status:
    Published
  11. Effect of Sn addition on the wettability of amorphous TiZrCuPdSn alloys on Ti-6Al-4V substrate

    Authors:
    K. Badura, A. Sypien, P. Fima
    Conference:
    AMT 2016 - XXI Physical Metallurgy and Materials Science Conference (year: 2016, pages: EP1), Publisher: BEL Studio Sp. z o.o.
    Date:
    conference 5-8.2016
    Status:
    Published
  12. Thermomechanical and structural characterization of TiAlV/TiCuZrPd/TiAlV interconnections

    Authors:
    Anna Sypien, Tomasz Czeppe, Grzegorz Garzel
    Conference:
    AMT 2016 - XXI Physical Metallurgy and Materials Science Conference (year: 2016, pages: BP13), Publisher: BEL Studio Sp. z o.o.
    Date:
    conference 5-8.06.2016
    Status:
    Published
  13. Microstructure, Phase Composition and Shear Strength of the TiAlV/TiCuZrPd/TiAlV Brazed Joints

    Authors:
    Anna Sypien1; Joanna Wojewoda-Budka1; Lidia Litynska-Dobrzynska1; Kamil Badura1
    Conference:
    TMS16 -145th annual meeting & Exhibition (year: 2016, pages: 19 - LL-87), Publisher: WILEY
    Date:
    conference 14-18.02.2016
    Status:
    Published
  14. Effect of aging temperature on the intermetallic phase stability after induction brazed of Ti-6Al-4V alloy with amorphous TiCuZrPd filler

    Authors:
    Anna Sypien, A.Wierzbicka-Miernik, K. Badura
    Conference:
    24th International Symposium on Metastable, Amorphous and Nanostructured Materials (year: 2017, pages: 264), Publisher: Arcady Zhukov
    Status:
    Accepted for publication

Book publications / chapters in book publications (1)

  1. Amorficzne stopy na osnowie tytanu jako perspektywiczny materiał lutowniczy

    Authors:
    Anna Sypień
    Book:
    Amorficzne stopy na osnowie tytanu jako perspektywiczny materiał lutowniczy (year: 2019, volume: 1, pages: 1-188), Publisher: Instytut Metalurgii i Inżynierii materiałowej PAN
    Status:
    Published

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Graphic design and implementation: Jakub Piotrowski