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Thio-modification of the new cyclization reaction of the Friedel-Crafts type and investigation of optoelectronic properties of thio-substituted (hetero)acenes

2013/11/B/ST5/01610

Keywords

Descriptors

  • ST5_23: Chemia organiczna

Panel

ST5 – Materials: materials synthesis, structure-properties relations, advanced and functional materials with designed properties, (macro)molecular architecture, material engineering

Host institution

Centrum Badań Molekularnych i Makromolekularnych PAN

Voivodeship: łódzkie

Other projects carried out by the institution »

Principal investigator (from the host institution)

prof. Piotr Bałczewski

Number of co-investigators in the project: 8

Call

OPUS 6 – announced on 2013-09-16

Amount awarded
1 222 074 PLN
Project start date
2014-08-22
Project end date
2017-11-21
Project duration
39 months (the same as in the proposal)
Project status
Project settled

Equipment purchased [PL]

  1. Bezozonowa lampa ksenonowa. Cost: 6 717 PLN
  2. Komputer wraz z oprogramowaniem systemowym i użytkowym. Cost: 6 000 PLN
  3. Oprogramowanie ChemDraw Standard (2 pcs). Cost: 1 500 PLN
  4. Oprogramowanie ChemOffice Pro 13.0 Siute. Cost: 5 500 PLN
  5. Oprogramowanie Origin wersja 9.1 (2 pcs). Cost: 5 000 PLN
  6. Pompa próżniowa. Cost: 13 000 PLN
  7. Rozszerzenie oprzyrządowania do posiadanego spektrofluorymetru Fluorolog-3: 1.1. Przystawka do pomiaru czasu życia fluorescencji metodą TCSPC. Cost: 165 000 PLN
  8. Rozszerzenie oprzyrządowania do posiadanego spektrofluorymetru Fluorolog-3: 1.2. Sfera całkująca dla spektrofluorymetru Fluorolog-3 z oprzyrządowaniem. Cost: 112 000 PLN
  9. Spektrofotometr UV-Vis ze sferą całkującą i oprzyrządowaniem (np. kuwety szklane i kwarcowe, komputer z monitorem LCD, zainstalowanym oprogramowaniem i drukarką). Cost: 86 000 PLN

Information in the final report

Publication in academic press/journals (6)

  1. Recent studies of the synthesis, functionalization, optoelectronic properties and applications of dibenzophospholes

    Authors:
    P. Hibner-Kulicka, J.A.Joule, J. Skalik, P.Bałczewski
    Academic press:
    RSC Advances (year: 2017, volume: 7, pages: 9194-9236), Publisher: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/C6RA26333J – link to the publication

  2. Synthesis of polycyclic (hetero)aromatic hydrocarbons via the Friedel–Crafts/Bradsher cyclization (na zaproszenie)

    Authors:
    A. Bodzioch , E. Kowalska , J. Skalik, P. Bałczewski
    Academic press:
    Chemistry of Heterocyclic Compounds (year: 2017, volume: 53(1), pages: 46346), Publisher: SpringerLink
    Status:
    Published
    DOI:
    10.1007/s10593-017-2015-y – link to the publication

  3. A selective removal of the secondary hydroxy group from ortho-dithioacetal-substituted diarylmethanols

    Authors:
    A.Czarnecka, E.Kowalska, A. Bodzioch, J. Skalik, M. Koprowski, K. Owsianik, P. Bałczewski
    Academic press:
    Beilstein Journal of Organic Chemistry (year: 2018, volume: 14, pages: 1229-1237), Publisher: Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.3762/bjoc.14.105 – link to the publication

  4. Efficient Synthesis of Bis(dibromomethyl)arenes as Important Precursors of Synthetically Useful Dialdehydes

    Authors:
    A. Bodzioch, K. Owsianik J. Skalik, E. Kowalska, A. Stasiak, E. Różycka-Sokołowska, B. Marciniak, P. Bałczewski
    Academic press:
    Synthesis (year: 2016, volume: 48, pages: 3509), Publisher: Georg Thieme Verlag Stuttgart · New York
    Status:
    Published
    DOI:
    10.1055/s-0035-1561651 – link to the publication

  5. Mono-Aryl/Alkylthio-Substituted (Hetero)acenes of Exceptional Thermal and Photochemical Stability by the Thio-Friedel-Crafts/Bradsher Cyclization Reaction

    Authors:
    P. Bałczewski, E. Kowalska, E. Różycka-Sokołowska, J. Skalik, K. Owsianik, M. Koprowski, B. Marciniak, D. Guziejewski, W. Ciesielski
    Academic press:
    Chemistry: A European Journal (year: 2019, volume: 25, pages: 14148-14161), Publisher: Wiley-VCH
    Status:
    Published
    DOI:
    10.1002/chem.201903027 – link to the publication

  6. Ultrasound-assisted synthesis of RO- and RS-substituted (hetero)acenes via oxo- and thio-Friedel-Crafts/Bradsher reactions

    Authors:
    P. Bałczewski, E. Kowalska, J. Skalik, M. Koprowski, K. Owsianik, E. Różycka-Sokołowska
    Academic press:
    Ultrasonics Sonochemistry (year: 2019, volume: 58, pages: bd), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.ultsonch.2019.104640 – link to the publication

Book publications / chapters in book publications (1)

  1. Quinquevalent phosphorus acids (QPA)

    Authors:
    Piotr Bałczewski, Joanna Skalik
    Book:
    Organophosphorus Chemistry: Volume 44 (year: 2015, volume: 44, pages: 289-377), Publisher: Royal Society of Chemistry
    Status:
    Published

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