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A novel continuous three-phase fixed-bed enzymatic reactor with hierarchically structured packing

2013/09/B/ST8/02420

Keywords

Descriptors

  • ST8_1: Inżynieria chemiczna, chemia techniczna, inżynieria środowiska, inżynieria sanitarna, inżynieria procesowa

Panel

ST8 – Production and processes engineering: modelling, product design, process design and control, construction methods and engineering, power units and systems

Host institution

Politechnika Śląska, Wydział Chemiczny

Voivodeship: śląskie

Other projects carried out by the institution »

Principal investigator (from the host institution)

prof. Andrzej Bolesław Jarzębski

Number of co-investigators in the project: 8

Call

OPUS 5 – announced on 2013-03-15

Amount awarded
954 760 PLN
Project start date
2014-03-21
Project end date
2017-09-20
Project duration
42 months (the same as in the proposal)
Project status
Project settled

Equipment purchased [PL]

  1. Apatrat do wyznaczania izoterm adsorpcji/desorpcji gazów w porowatych materiałach stałych w niskich temperaturach. Cost: 250 000 PLN
  2. Kolumny chromatograficzne (2 pcs). Cost: 20 000 PLN
  3. Mieszadło mechaniczne.
  4. Pompa dozująca. Cost: 10 000 PLN
  5. Przenośny komputer z systemem operacyjnym. Cost: 5 000 PLN
  6. Wysokosprawna pompa dozująca. Cost: 65 000 PLN
  7. detektor refraktometryczny (pokrycie części kosztów).
  8. piec rurowy. Cost: 15 375 PLN
  9. pomyłka przy wypełnianiu tabeli.
  10. reaktor typu SpinChem.
  11. waga analityczna. Cost: 9 499 PLN

Information in the final report

Publication in academic press/journals (9)

  1. Novel hierarchically structured packing for rotating bed reactors. proof-of-concept and viability studies in the enzyme-catalysed reactions

    Authors:
    K. Szymańska, K. Odrozek, A. Zniszczoł, W. Pudło, J. Bryjak, A. Jarzębski
    Academic press:
    Materiały Konferencyjne 22. Ogólnopolskiej Konferencji Inżynierii Chemicznej i Procesowej (year: 2016, volume: brak, pages: 1403-1407), Publisher: Exall- ISBN 978-83-61997-73-3
    Status:
    Published

  2. Continuous hierarchically structured multichannel microreactors – engineering and performance

    Authors:
    K. Szymańska, J. Mrowiec-Białoń, A. Jarzębski
    Academic press:
    Materiały Konferencyjne 22. Ogólnopolskiej Konferencji Inżynierii Chemicznej i Procesowej (year: 2016, volume: brak, pages: 1399-1402), Publisher: Exall- ISBN 978-83-61997-73-3
    Status:
    Published

  3. Aerobic enzymatic oxidation of benzoic acid derivatives in a rotating bed reactor with hierarchically structured packing

    Authors:
    K. Odrozek, K. Szymańska, M. Lewańczuk, G. Dzido, W. Pudło, J. Bryjak, A. Jarzębski
    Academic press:
    Przemysł Chemiczny (year: 2017, volume: 96, pages: 2446-2449), Publisher: Wydawnictwo SIGMA-NOT
    Status:
    Published
    DOI:
    10.15199/62.2017.12.7 – link to the publication

  4. A robust chemo-enzymatic lactone synthesis using acyltransferase from Mycobacterium smegmatis

    Authors:
    A. Drożdż, U. Hanefeld, K. Szymańska, A. Jarzębski, A. Chrobok
    Academic press:
    Catalysis Communications (year: 2016, volume: 81, pages: 37-40), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.catcom.2016.03.021 – link to the publication

  5. Silica-supported chlorometallate(III) ionic liquids as recyclable catalysts for Diels-Alder reaction under solventless conditions

    Authors:
    K. Matuszek, A. Chrobok, P. Latos, M. Markiton, K. Szymańska, A. Jarzębski, M. Swadźba-Kwaśny
    Academic press:
    Catalysis Science & Technology (year: 2016, volume: 6, pages: 8129-8137), Publisher: The Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/c6cy01771a – link to the publication

  6. Batch and in-flow kinetic resolution of racemic 1-(N-acylamino)alkylphosphonic and 1-(N-acylamino)alkylphosphinic acids and their esters using immobilized penicillin G acylase

    Authors:
    K. Zielińska, K. Szymańska, A. Jarzębski, R. Mazurkiewicz
    Academic press:
    Tetrahedron: Asymmetry (year: 2017, volume: 28, pages: 146-152), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.tetasy.2016.11.007 – link to the publication

  7. A novel hierarchically structured siliceous packing to boost the performance of rotating bed enzymatic reactors

    Authors:
    K. Szymanska, K. Odrozek, A. Zniszczoł, W. Pudło, A. Jarzębski
    Academic press:
    Chemical Engineering Journal (year: 2017, volume: 315, pages: 18-24), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.cej.2016.12.131 – link to the publication

  8. Kinetics of enantiomerically enriched synthesis of solketal esters using native and sba-15 supported P. fluorescens lipase

    Authors:
    A. Zniszczoł, K. Szymańska, J. Kocurek, J. Bryjak, K. Walczak, A. Jarzębski
    Academic press:
    Chemical and Process Engineering (year: 2017, volume: 38 (2), pages: 209-215), Publisher: TECHNICAL UNIV WROCLAW
    Status:
    Published
    DOI:
    10.1515/cpe-2017-0016 – link to the publication

  9. Synthesis and Textural Characterization of Mesoporous and Meso-/Macroporous Silica Monoliths Obtained by Spinodal Decomposition

    Authors:
    A. Galarneau, Z. Abid, B. Said, Y. Didi, K. Szymanska, A. Jarzębski, F. Tancret, H. Hamaizi, A. Bengueddach, F. Di Renzo, F. Fajula
    Academic press:
    Inorganics (year: 2016, volume: 4(2), pages: 9), Publisher: MDPI
    Status:
    Published
    DOI:
    10.3390/inorganics4020009 – link to the publication

Articles in post-conference publications (5)

  1. Multichanel monolithic enzymatic microreactors-paving the way to new robust technologies

    Authors:
    K.Szymańska, J. Byjak, A. Jarzębski
    Conference:
    3rd Symposium on biotransformations for pharmaceutical and cosmetic industry (year: 2016, pages: 27), Publisher: Instytut Chemii Organicznej PAN
    Date:
    conference 30.06.2016-02.07.2016
    Status:
    Published

  2. Continuous-flow transition metal modified silica-based monolithic microreactors

    Authors:
    A. Koreniuk, K. Maresz, J. Malinowski, J. Mrowiec-Białoń, A. Jarzębski
    Conference:
    4th Zing Continuous Flow Chemistry Conference (year: 2016, pages: 67), Publisher: 4th Zing Continuous Flow Chemistry Conference
    Date:
    conference 25-28th April 2016
    Status:
    Published

  3. Reaktory mikrofluidalne – właściwości, inżynieria, zastosowanie

    Authors:
    K. Szymańska, A. Zniszczoł, K. Odrozek, W. Pudło, A. Koreniuk, K. Maresz, J. Kocurek, J. Mrowiec-Białoń, A. Jarzębski
    Conference:
    8. Kongres Technologii Chemicznej (year: 2015, pages: 122), Publisher: Politechnika Rzeszowska
    Date:
    conference 30.08-04.09. 2015r.
    Status:
    Published

  4. Continuous hierarchically structured multichannel microreactors – engineering and performance

    Authors:
    K. Szymańska, J. Mrowiec-Białoń, A. Jarzębski
    Conference:
    22. Ogólnopolskiej Konferencji Inżynierii Chemicznej i Procesowej (year: 2016, pages: 223), Publisher: Exall, Łódź ISBN 978-83-61997-73-3
    Date:
    conference 5-9.09.2016
    Status:
    Published

  5. Novel hierarchically structured packing for rotating bed reactors. proof-of-concept and viability studies in the enzyme-catalysed reactions

    Authors:
    K. Szymańska, K. Odrozek, A. Zniszczoł, W. Pudło, J. Bryjak, A. Jarzębski
    Conference:
    22. Ogólnopolskiej Konferencji Inżynierii Chemicznej i Procesowej (year: 2016, pages: 224), Publisher: Exall, Łódź ISBN 978-83-61997-73-3
    Date:
    conference 5-9.09.2016
    Status:
    Published

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