Projects funded by the NCN

Information on the principal investigator and host institution

Information of the project and the call

Keywords

Equipment

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New catalysts containing Zr, Nb, Mo, Au, Pt loaded on porous supports for low-energy processes for fine chemicals production

2011/01/B/ST5/00847

Keywords:

methanol glycerol hydrocarbons oxidation MCM-36 MCM-56 zeolites MCF foams

Descriptors:

  • ST5_6: Porous materials, ceramics, glasses
  • ST5_3: Surface modification
  • ST5_18:

Panel:

ST5 - Materials: materials synthesis, structure-properties relations, advanced and functional materials with designed properties, (macro)molecular architecture, material engineering

Host institution :

Uniwersytet im. Adama Mickiewicza w Poznaniu, Wydział Chemii

woj. wielkopolskie

Other projects carried out by the institution 

Principal investigator (from the host institution):

prof. Maria Ziółek 

Number of co-investigators in the project: 10

Call: OPUS 1 - announced on 2011-03-15

Amount awarded: 750 000 PLN

Project start date (Y-m-d): 2011-12-12

Project end date (Y-m-d): 2014-12-11

Project duration:: 36 months (the same as in the proposal)

Project status: Project settled

Equipment purchased [PL]

  1. Zestaw reaktorów do prowadzenia reakcji w fazie ciekłej (15 000 PLN)
  2. Autoklaw - reaktor ciśnieniowy (75 000 PLN)
  3. Chromatograf gazowy z MS (250 000 PLN)
  4. Pompa infuzyjna (15 000 PLN)

Information in the final report

  • Publication in academic press/journals (21)
  • Articles in post-conference publications (26)
  1. Real-Time Raman Monitoring and Control of the Catalytic Acetalization of Glycerol with Acetone over Modified Mesoporous Cellular Foams
    Authors:
    V. Calvino-Casilda, K. Stawicka, M. Trejda, M. Ziolek, M.A. Bañares
    Academic press:
    The Journal of Physical Chemistry C (rok: 2014, tom: 118, strony: 10780-10791), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp500651e - link to the publication
  2. Search for reactive intermediates in catalytic oxidation with hydrogen peroxide over amorphous niobium(V) and tantalum(V) oxides
    Authors:
    M. Ziolek, I. Sobczak, P. Decyk, K. Sobanska, P. Pietrzyk, Z. Sojka
    Academic press:
    Applied Catalysis B: Environmental (rok: 2015, tom: 164, strony: 288–296), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.apcatb.2014.09.024 - link to the publication
  3. Surface and catalytic properties of Ce, Zr, Au, Cu modified SBA-15
    Authors:
    P. Kaminski, M. Ziolek
    Academic press:
    Journal of Catalysis (rok: 2014, tom: 312, strony: 249-262), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.jcat.2014.02.005 - link to the publication
  4. Surface properties and catalytic performance of Pt-Ag supported on silica – the effect of preparation methods
    Authors:
    J. Czaplinska, P. Decyk, M. Ziolek
    Academic press:
    Applied Catalysis A: General (rok: 2015, tom: xxx, strony: xxx), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.apcata.2014.12.054 - link to the publication
  5. The ability of Nb2O5 and Ta2O5 to generate active oxygen in contact with hydrogen peroxide
    Authors:
    Maria Ziolek, Izabela Sobczak, Piotr Decyk, Lukasz Wolski
    Academic press:
    Catalysis Communications (rok: 2013, tom: 37, strony: 85–91), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.catcom.2013.03.032 - link to the publication
  6. The production of biofuels additives on sulphonated MCF materialsmodified with Nb and Ta—Towards efficient solid catalysts of esterification
    Authors:
    Katarzyna Stawicka, Maciej Trejda, Maria Ziolek
    Academic press:
    Applied Catalysis A: General (rok: 2013, tom: 467, strony: 325– 334), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.apcata.2013.07.036 - link to the publication
  7. The role of Nb in the formation of sulphonic species in SBA-15 and MCF functionalised with MPTMS
    Authors:
    M. Trejda, K. Stawicka, M. Ziolek
    Academic press:
    Catalysis Today (rok: 2012, tom: 192, strony: 130-135), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.cattod.2012.02.042 - link to the publication
  8. Amino-grafted mesoporous materials based on MCF structure involved in the quinoline synthesis. Mechanistic insights
    Authors:
    A. Smuszkiewicz, J. López-Sanz, E. Pérez-Mayoral, E. Soriano, I. Sobczak, M. Ziolek, R.M. Martín-Aranda, A.J. López-Peinadoa
    Academic press:
    Journal of Molecular Catalysis A: Chemical (rok: 2013, tom: 378, strony: 38– 46), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.molcata.2013.05.017 - link to the publication
  9. Comparative study of Zr, Nb, Mo containing SBA-15 grafted with amino-organosilanes
    Authors:
    M. Olejniczak, M. Ziolek
    Academic press:
    Microporous and Mesoporous Materials (rok: 2014, tom: 196, strony: 243 – 253), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.micromeso.2014.05.018 - link to the publication
  10. FTIR spectroscopic study of CO oxidation on bimetallic catalysts
    Authors:
    P. Kaminski, M. Ziolek, B. Campo, M. Daturi
    Academic press:
    Catalysis Today (rok: 2015, tom: 243, strony: 218-227), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.cattod.2014.08.035 - link to the publication
  11. Niobiosilica materials as attractive supports for Sb-V-O catalysts
    Authors:
    H. Golinska-Mazwa, E. Rojas, R. Lopez-Medina, M. Ziolek, M.A. Banares, M.O. Guerrerro-Perez
    Academic press:
    Topics in Catalysis (rok: 2012, tom: 55, strony: 837-845), Wydawca: Springer
    Status:
    Published
    DOI:
    10.1007/s11244-012-9855-6 - link to the publication
  12. The role of pillaring in MCM-22 on the dispersion of noble metals and catalytic activity
    Authors:
    A. Wojtaszek-Gurdak, I. Sobczak, K. Grzelak, M. Ziolek, U. Hartfelder, J. A. van Bokhoven
    Academic press:
    Materials Research Bulletin (rok: 2015, tom: XX, strony: XX), Wydawca: Elsevier
    Status:
    Submitted
    DOI:
    brak - link to the publication
  13. Au containing mesostructured cellular foams NbMCF and ZrMCF in selective oxidation of methanol to formaldehyde
    Authors:
    I. Sobczak, M. Kozlowska, M. Ziolek
    Academic press:
    Journal of Molecular Catalysis A: Chemical (rok: 2014, tom: 390, strony: 114-124), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.molcata.2014.03.015 - link to the publication
  14. Comparative study of MCM-22 and MCM-56 modified with molybdenum - Impact of the metal on acidic and oxidative properties of zeolites
    Authors:
    A. Wojtaszek-Gurdak, M. Trejda, D. Kryszak, M. Ziolek
    Academic press:
    Microporous and Mesoporous Materials (rok: 2014, tom: 197, strony: 185 - 193), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.micromeso.2014.06.011 - link to the publication
  15. Zeolite MCM-22 modified with Au and Cu for catalytic total oxidation of methanol and carbon monoxide
    Authors:
    P. Kaminski, I. Sobczak, P. Decyk, M. Ziolek, W.J. Roth, B. Campo, M. Daturi
    Academic press:
    The Journal of Physical Chemistry C (rok: 2013, tom: 117, strony: 2147-2159), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp310505y - link to the publication
  16. Bifunctional mesoporous MCF materials as catalysts in the Friedländer condensation
    Authors:
    A. Smuszkiewicz, E. Pérez-Mayoral, E. Soriano, I. Sobczak, M. Ziolek,
    Academic press:
    Catalysis Today (rok: 2013, tom: 218– 219, strony: 70– 75), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.cattod.2013.04.034 - link to the publication
  17. Esterification processes based on functionalized mesoporous solids
    Authors:
    M. Trejda, B. Pokora, M. Ziolek
    Academic press:
    Catalysis Today (rok: 2015, tom: XXX, strony: XXX), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.cattod.2014.11.034 - link to the publication
  18. New phospho-silicate and niobo-phospho-silicate MCF materials modified with MPTMS - Structure, surface and catalytic properties
    Authors:
    Katarzyna Stawicka, Maciej Trejda, Maria Ziolek
    Academic press:
    Microporous and Mesoporous Materials (rok: 2013, tom: 181, strony: 88-98), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.micromeso.2013.07.002 - link to the publication
  19. Relationship between basicity, reducibility and partial oxidation properties of chromium containing MCM-41
    Authors:
    M. Trejda, M. Bryś, M. Ziolek
    Academic press:
    RSC Advances (rok: 2014, tom: 4, strony: 62940), Wydawca: RSC
    Status:
    Published
    DOI:
    10.1039/c4ra10336j - link to the publication
  20. Nb and Zr modified MWW zeolites - characterisation and catalytic activity
    Authors:
    A. Wojtaszek-Gurdak, M. Ziolek
    Academic press:
    RSC Advances (rok: 2015, tom: 5, strony: 22326 - 22333), Wydawca: RSC
    Status:
    Published
    DOI:
    10.1039/c5ra00411j - link to the publication
  21. Organosilanes affecting the structure and formation of mesoporous cellular foams
    Authors:
    K. Stawicka, I. Sobczak, M. Trejda, B. Sulikowski, M. Ziolek
    Academic press:
    Microporous and Mesoporous Materials (rok: 2012, tom: 155, strony: 143-152), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.micromeso.2012.01.026 - link to the publication
  1. Comparative study of Zr, Nb, Mo containing SBA-15 grafted with amino-organosilanes
    Authors:
    M. Olejniczak, M. Ziolek
    Conference:
    8th International Symposium on Group Five Elements (rok: 2014, ), Wydawca: Organizing Committee; Book of Abstracts
    Data:
    konferencja 24-27 czerwca
    Status:
    Published
  2. Isomorphous substitution of transition metals into zeolites as a tool for creation of new catalysts
    Authors:
    14.F. Tielens, A. Wojtaszek, M. Trejda, G. Skara, F. de Proft. M. Calatayud, M. Ziolek, S. Dzwigaj
    Conference:
    XIth European Congress on Catalysis (EuropaCat) (rok: 2013, ), Wydawca: Organizing Committee; Book of Abstracts
    Data:
    konferencja 01–06 września 2013
    Status:
    Published
  3. Mesoporous mixed oxides of cerium and zirconium modified with Au andf Cu - synthesis, characterization and performance in glycerol oxidation
    Authors:
    J.A. van Bekhoven, P. Kaminski, M. Ziolek
    Conference:
    SCS FAll Meeting 2014 (rok: 2014, ), Wydawca: Organizing Committee, Book of Poster Abstracts
    Data:
    konferencja 11 września
    Status:
    Published
  4. Sposób zagospodarowania glicerolu - nowe heterogeniczne katalizatory estryfikacji glicerolu
    Authors:
    M. Trejda, K. Stawicka, M. Ziółek
    Conference:
    55 Zjazd Polskiego Towarzystwa Chemicznego i Stowarzyszenia Inżynierów i Techników Przemysłu Chemicznego (rok: 2012, ), Wydawca: Polskie Towarzystwo Chemiczne; ISBN: 978-83-60988-12-1
    Data:
    konferencja 16-20 września 2012
    Status:
    Published
  5. The influence of Ce, Zr, Au, Cu modifiers of SBA-15 on acidic and redox properties in methanol oxidation
    Authors:
    P. Kaminski, M. Ziolek
    Conference:
    6th FEZA Conference (rok: 2014, ), Wydawca: Organizing Committee; Book of Abstracts
    Data:
    konferencja 8-11 września
    Status:
    Published
  6. The role of niobium species in heterogeneous catalysis
    Authors:
    M. Ziolek
    Conference:
    11th Pannonian International Symposium on Catalysis, Obergurgl, Austria (rok: 2012, ), Wydawca: Universitatszentrum, Obergurgl, Tyrol, Austria; EAN-Code 9783900554712; ISBN 97-8-3-900554-71-2
    Data:
    konferencja 3-7 września 2012
    Status:
    Published
  7. Comparative study of MCM-22 and MCM-56 modified with niobium, zirconium, and molybdenum
    Authors:
    A. Wojtaszek-Gurdak, M. Trejda, D. Kryszak, M. Ziolek
    Conference:
    12 th Pannonian Symposium on Catalysis (rok: 2014, ), Wydawca: Institute of Chemical Technology
    Data:
    konferencja 16-20 września
    Status:
    Published
  8. New SBA-15 mesoporous molecular sieves containing zirconium, niobium and molybdenum modified with organosilanes
    Authors:
    M. Bartoszewska, I. Sobczak, M. Ziolek
    Conference:
    School of Molecular Sieves (rok: 2013, ), Wydawca: J Heyrovsky Institute of Physical Chemistry of the ASCR; ISBN 978-80-87351-23-9
    Data:
    konferencja 10-12 marca 2013
    Status:
    Published
  9. The role of basicity in methanol oxidation - relationship between basicity and redox properties of Cr containing MCM-41
    Authors:
    M. Trejda, M. Bryś, M. Ziolek
    Conference:
    6th FEZA Conference (rok: 2014, ), Wydawca: Organizing Committee; Book of Abstracts
    Data:
    konferencja 8-11 września
    Status:
    Published
  10. FTIR operando system used for PROX study on MCM-22 zeolites modified with gold and copper
    Authors:
    P. Kaminski, I. Sobczak, P. Decyk, M. Ziolek, W.J. Roth, B. Campo, M. Daturi
    Conference:
    School of Molecular Sieves (rok: 2013, ), Wydawca: J Heyrovsky Institute of Physical Chemistry of the ASCR; ISBN 978-80-87351-23-9
    Data:
    konferencja 10-12 marca 2013
    Status:
    Published
  11. In search of effective catalysts for triacetylglycerol production
    Authors:
    M. Bartoszewska, M. Trejda, M. Ziółek
    Conference:
    XLIV Ogólnopolskie Kolokwium Katalityczne, Kraków (rok: 2012, ), Wydawca: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera, PAN; ISBN: 978-83-60-514-15-3
    Data:
    konferencja 14-16 marca 2012
    Status:
    Published
  12. Modification of micro- and mesoporous molecular sieves and preparation of mixed metal oxides in order to obtain catalysts active in oxidation processes
    Authors:
    M. Ziółek, I. Sobczak, M. Trejda, P. Decyk, H. Golińska-Maźwa, A. Wojtaszek
    Conference:
    XLIV Ogólnopolskie Kolokwium Katalityczne, Kraków (rok: 2012, ), Wydawca: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera, PAN; ISBN: 978-83-60-514-15-3
    Data:
    konferencja 14-16 marca 2012
    Status:
    Published
  13. Modified MCF catalysts active in glycerol esterification
    Authors:
    K. Stawicka, M. Trejda, M. Ziółek
    Conference:
    XLIV Ogólnopolskie Kolokwium Katalityczne, Kraków (rok: 2012, ), Wydawca: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera, PAN; ISBN: 978-83-60-514-15-3
    Data:
    konferencja 14-16 marca 2012
    Status:
    Published
  14. NbMCF and ZrMCF mesostructured cellular foams as new supports for gold – surface and oxidative properties
    Authors:
    I. Sobczak, M. Kozłowska, M. Ziolek
    Conference:
    8th International Symposium on Group Five Elements (rok: 2014, ), Wydawca: Organizing Committee; Book of Abstracts
    Data:
    konferencja 24-27 czerwca
    Status:
    Published
  15. Surface properties of molybdenum modified HMCM-22 and HMCM-56 zeolites - comparative study
    Authors:
    A. Wojtaszek, A. Zarecki, M. Ziolek
    Conference:
    School of Molecular Sieves (rok: 2013, ), Wydawca: J Heyrovsky Institute of Physical Chemistry of the ASCR; ISBN 978-80-87351-23-9
    Data:
    konferencja 10-12 marca 2013
    Status:
    Published
  16. Towards efficient catalysts of esterification - metal impact on sulphonic species formation
    Authors:
    K. Jenerowicz, M. Trejda, K. Stawicka, M. Ziolek
    Conference:
    XLV Ogólnopolskie Kolokwium Katalityczne (rok: 2013, ), Wydawca: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera, PAN; ISBN 78-83-60514-18-4
    Data:
    konferencja 13-15 marca 2013
    Status:
    Published
  17. Comparative study of MCM-22 and MCM-56 modified with molybdenum - metal impact on acidic and redox properties
    Authors:
    A. Wojtaszek-Gurdak, M. Trejda, D. Kryszak, M. Ziolek
    Conference:
    6th FEZA Conference (rok: 2014, ), Wydawca: Organizing Committee; Book of Abstracts
    Data:
    konferencja 8-11 września
    Status:
    Published
  18. Insight into the interaction of hydrogen peroxide with niobium(V) and tantalum(V) oxides
    Authors:
    M. Ziolek, I. Sobczak, P. Decyk, K. Domaradzka, P. Pietrzyk, Z. Sojka
    Conference:
    8th International Symposium on Group Five Elements (rok: 2014, ), Wydawca: Organizing Committee; Book of Abstracts
    Data:
    konferencja 24-27 czerwca
    Status:
    Published
  19. Mesostructured cellular foams (MCF) doped with niobium or zirconium as a new silicate matrix for gold
    Authors:
    M. Kozlowska, I. Sobczak, M. Ziolek
    Conference:
    XLV Ogólnopolskie Kolokwium Katalityczne (rok: 2013, ), Wydawca: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera, PAN; ISBN78-83-60514-18-4
    Data:
    konferencja 13-15 marca 2013
    Status:
    Published
  20. SBA-15 containing zirconium, niobium and molybdenum grafted with aminosilanes – texture, surface and catalytic properties
    Authors:
    M. Olejniczak, M. Ziolek
    Conference:
    School of Molecular Sieves (rok: 2014, ), Wydawca: J.Heyrovsky Insitute of Physical Chemistry of the ASCR,v.v.i.; Program Book of Abstracts
    Data:
    konferencja 17-18 marca
    Status:
    Published
  21. The Ability of Niobium and Tantalum Oxides and Metallo-silicates to Generate Catalytic Active Oxygen in Contact with Hydrogen Peroxide
    Authors:
    M. Ziolek, I. Sobczak, P. Decyk, L. Wolski, K. Stawicka, M. Trejda
    Conference:
    XIth European Congress on Catalysis (EuropaCat) (rok: 2013, ), Wydawca: Organizing Committee; Book of Abstracts
    Data:
    konferencja 01–06 września 2013
    Status:
    Published
  22. Comparative study of MCM-22 and MCM-56 modified with niobium and zirconium - metal impact on acidic and redox properties
    Authors:
    A. Wojtaszek - Gurdak, A. Nowak, M. Ziolek
    Conference:
    8th International Symposium on Group Five Elements (rok: 2014, ), Wydawca: Organizing Committee; Book of Abstracts
    Data:
    konferencja 24-27 czerwca
    Status:
    Published
  23. Interactions of different oxidants with amorphous and crystalline Group Five Metal Oxides
    Authors:
    Ł. Wolski, I. Sobczak, P. Decyk, M. Ziółek
    Conference:
    XLIV Ogólnopolskie Kolokwium Katalityczne, Kraków (rok: 2012, ), Wydawca: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera, PAN; ISBN: 978-83-60-514-15-3
    Data:
    konferencja 14-16 marca 2012
    Status:
    Published
  24. MCM-22 zeolites modified with gold and copper - the physicochemical properties and application in CO oxidation
    Authors:
    P. Kamiński, I. Sobczak, M. Ziółek, M. Daturi, W. Roth
    Conference:
    XLIV Ogólnopolskie Kolokwium Katalityczne, Kraków (rok: 2012, ), Wydawca: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera, PAN; ISBN: 978-83-60-514-15-3
    Data:
    konferencja 14-16 marca 2012
    Status:
    Published
  25. Modified MCF catalysts dedicated for acetic acid esterification
    Authors:
    K. Stawicka, M. Trejda, M. Ziolek
    Conference:
    11th Pannonian International Symposium on Catalysis, Obergurgl, Austria (rok: 2012, ), Wydawca: Universitatszentrum, Obergurgl, Tyrol, Austria; EAN-Code 9783900554712; ISBN 97-8-3-900554-71-2
    Data:
    konferencja 3-7 września 2012
    Status:
    Published
  26. New Ag-Cu bimetallic system based on SBA-15 - physicochemical and catalytic properties
    Authors:
    J. Czaplinska, I. Sobczak, M. Ziolek
    Conference:
    XLV Ogólnopolskie Kolokwium Katalityczne (rok: 2013, ), Wydawca: Instytut Katalizy i Fizykochemii Powierzchni im. Jerzego Habera, PAN; ISBN78-83-60514-18-4
    Data:
    konferencja 13-15 marca 2013
    Status:
    Published

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