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Study of the oxygen footprint and its significance in the kesterite Cu2ZnSnS4 semiconductor for next generation photovoltaic cells

2020/37/B/ST5/00151

Keywords:

photovoltaics kesterite Cu2ZnSnS4 semiconductor preparation structure spectroscopic properties adventitious oxidation oxygen groups oxygen content determination

Descriptors:

  • ST5_010:

Panel:

ST5 - Materials: materials synthesis, structure-properties relations, advanced and functional materials with designed properties, (macro)molecular architecture, material engineering

Host institution :

Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie, Wydział Energetyki i Paliw

woj. małopolskie

Other projects carried out by the institution 

Principal investigator (from the host institution):

prof. Jerzy Franciszek Janik 

Number of co-investigators in the project: 3

Call: OPUS 19 - announced on 2020-03-16

Amount awarded: 1 184 400 PLN

Project start date (Y-m-d): 2021-01-11

Project end date (Y-m-d): 2024-05-10

Project duration:: 40 months (the same as in the proposal)

Project status: Project settled

Project description

Download the project description in a pdf file

Note - project descriptions were prepared by the authors of the applications themselves and placed in the system in an unchanged form.

Information in the final report

  • Publication in academic press/journals (6)
  • Articles in post-conference publications (31)
  1. Thermogravimetric/thermal–mass spectroscopy insight into oxidation propensity of various mechanochemically made kesterite Cu2ZnSnS4 nanopowders
    Authors:
    Katarzyna Lejda, Janusz Partyka, Jerzy F. Janik
    Academic press:
    Materials (rok: 2024, tom: 17(6), strony: No. 1232 (1-17)), Wydawca: MDPI
    Status:
    Published
    DOI:
    10.3390/ma17061232 - link to the publication
  2. Oxygen aspects in high-pressure and high-temperature sintering of nanocrystalline powders of semiconductor kesterite Cu2ZnSnS4
    Authors:
    Katarzyna Lejda, Jerzy F. Janik, Marcin Perzanowski, Svitlana Stelmakh, Bogdan Pałosz
    Academic press:
    International Journal of Molecular Sciences (rok: 2023, tom: 24(4), strony: 3158 (1-18)), Wydawca: MDPI
    Status:
    Published
    DOI:
    10.3390/ijms24043159 - link to the publication
  3. Long-term oxidation susceptibility in ambient air of the semiconductor kesterite Cu2ZnSnS4 nanopowders made by mechanochemical synthesis method
    Authors:
    K. Lejda, M. Ziąbka, Z. Olejniczak, J.F. Janik
    Academic press:
    Materials (rok: 2023, tom: 16(18), strony: 6160 (1-17)), Wydawca: MDPI
    Status:
    Published
    DOI:
    10.3390/ma16186160 - link to the publication
  4. Oxygen aspects in high-pressure and high-temperature sintering of semiconductor kesterite Cu2ZnSnS4 nanopowders prepared by a mechanochemically-assisted synthesis method
    Authors:
    Katarzyna Lejda, Jerzy F. Janik, Marcin Perzanowski, Svitlana Stelmakh, Bogdan Pałosz
    Academic press:
    International Journal of Molecular Sciences (rok: 2023, tom: 24(4), strony: 3158 (1-18)), Wydawca: MDPI
    Status:
    Published
    DOI:
    10.3390/ijms24043159 - link to the publication
  5. Long-term oxidation susceptibility in ambient air of the semiconductor kesterite Cu2ZnSnS4 nanopowders made by mechanochemical synthesis method
    Authors:
    K. Lejda, M. Ziąbka, Z. Olejniczak, J.F. Janik
    Academic press:
    Materials (rok: 2023, tom: 16(18), strony: 6160 (1-17)), Wydawca: MDPI
    Status:
    Published
    DOI:
    10.3390/ma16186160 - link to the publication
  6. Oxygen aspects in high-pressure and high-temperature sintering of nanocrystalline powders of semiconductor kesterite Cu2ZnSnS4
    Authors:
    Katarzyna Lejda, Jerzy F. Janik, Marcin Perzanowski, Svitlana Stelmakh, Bogdan Pałosz
    Academic press:
    International Journal of Molecular Sciences (rok: 2023, tom: 24(4), strony: 3158 (1-18)), Wydawca: MDPI
    Status:
    Published
    DOI:
    10.3390/ijms24043159 - link to the publication
  1. Infrared FT-IR insight into prolonged exposure to ambient air of semiconductor kesterite Cu2ZnSnS4 nanopowders prepared via mechanochemical synthesis route
    Authors:
    Jerzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2023, tom: International Conference on Materials Science and Engineering - Materials Oceania 2023, strony: 67-68), Wydawca: PRISM, Nagoya University, Japan
    Data:
    konferencja 26-29 wrzesień, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  2. Solid-state 65Cu/119Sn MAS NMR study of prolonged oxidation in ambient air of semiconductor kesterite CuZnSnS4 nanopowders
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Zbigniew Olejniczak
    Conference:
    Book of Abstracts (rok: 2023, tom: SIPS 2023 - sustainability through science & technology, strony: 99), Wydawca: Canada : FLOGEN Stars OUTREACH
    Data:
    konferencja 27 November-1 December, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  3. Oxygen-bearing species evolved in TGA/DTA/MS experiments for nanopowders of semiconductor kesterite Cu2ZnSnS4 prepared from the {2Cu+Zn+Sn+4S} system
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Janusz Partyka
    Conference:
    Book of abstracts (rok: 2022, tom: 4th World Nanotechnology Summit, strony: str. 34), Wydawca: Phronesis
    Data:
    konferencja 19-20 September 2022
    Status:
    Published
  4. TGA/DTA/MS insight into decomposition of semiconductor kesterite Cu2ZnSnS4 nanopowders prepared via mechanochemically-assisted synthesis method from in-situ made Zn/Sn copper alloys
    Authors:
    Jerzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2024, tom: 5th International Conference on Nanomaterials, Nanofabrication and Nanocharacterization - NANOMACH 2024, strony: 33), Wydawca: Gebze University oraz Kocaeli University - Turcja
    Data:
    konferencja 18-24 April, 2024
    Status:
    Published
    DOI:
    https://doi,org/brak - link to the publication
  5. Oxygen aspect in high-pressure and high-temperature sintering of nanocrystalline powders of semiconductor kesterite Cu2ZnSnS4
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Svitlana Stelmakh, Bogdan Palosz
    Conference:
    Book of abstracts (rok: 2022, tom: 4th World Nanotechnology Summit, strony: str. 33), Wydawca: Phronesis
    Data:
    konferencja 19-20 September 2022
    Status:
    Published
  6. Convenient two-step analysis of adventitious surface-bound and bulk oxygen contents in the metal and sulfide precursors to semiconductor kesterite Cu2ZnSnS4
    Authors:
    H. Osip, K. Lejda, M. Drygaś, J.F. Janik
    Conference:
    Book of Astracts - NN21, 18th International Conference on Nanosciences and Nanotechnologies (dostępny po zalogowaniu) (rok: 2021, tom: NN21 - 18th Int. Conf. on Nano, strony: 179), Wydawca: Aristotle University of Thessaloniki, Thessaloniki, Greece
    Data:
    konferencja 6-9 July 2021
    Status:
    Published
  7. Effect of kesterite oxidation in the ambient air on its semiconductor properties – study of kesterite nanopowders from three different precursor systems
    Authors:
    Katarzyna Lejda, Jerzy F. Janik
    Conference:
    Book of Abstracts (rok: 2023, tom: FEMS EUROMAT23 : [Materials Science and Technology in Europe], strony: 1355), Wydawca: Germany : German Materials Society - DGM e. V.
    Data:
    konferencja 3-7 wrzesień, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  8. Oxygen aspect in high-pressure and high-temperature sintering of nanocrystalline powders of semiconductor kesterite Cu2ZnSnS4
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Svitlana Stelmakh, Bogdan Palosz
    Conference:
    Book of abstracts (rok: 2022, tom: 4th World Nanotechnology Summit, strony: str. 33), Wydawca: Phronesis
    Data:
    konferencja 19-20 September 2022
    Status:
    Published
  9. 3 months insight into the oxidation in air of semiconductor Cu2ZnSnS4 nanopowders made via high energy ball milling of copper alloys
    Authors:
    erzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2023, tom: 4 th International Congress on Advanced Materials Science and Engineering, strony: 184), Wydawca: Vienna : International Science and Technology Conference Institute (ISTCI)
    Data:
    konferencja 17-21 marzec, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  10. Convenient two-step analysis of adventitious surface-bound and bulk oxygen contents in the metal and sulfide precursors to semiconductor kesterite Cu2ZnSnS4
    Authors:
    H. Osip, K. Lejda, M. Drygaś, J.F. Janik
    Conference:
    Book of Astracts - NN21, 18th International Conference on Nanosciences and Nanotechnologies (dostępny po zalogowaniu) (rok: 2021, tom: NN21 - 18th Int. Conf. on Nano, strony: 179), Wydawca: Aristotle University of Thessaloniki, Thessaloniki, Greece
    Data:
    konferencja 6-9 July 2021
    Status:
    Published
  11. 3 months insight into the oxidation in air of semiconductor Cu2ZnSnS4 nanopowders made via high energy ball milling of copper alloys
    Authors:
    erzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2023, tom: 4 th International Congress on Advanced Materials Science and Engineering, strony: 184), Wydawca: Vienna : International Science and Technology Conference Institute (ISTCI)
    Data:
    konferencja 17-21 marzec, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  12. 6 month-long insight into the oxidation in air of semiconductor Cu2ZnSnS4 nanopowders
    Authors:
    Katarzyna Lejda, Jerzy F. Janik
    Conference:
    Book of Abstracts (rok: 2023, tom: FEMS EUROMAT23 : [materials science and technology in Europe], strony: 1343), Wydawca: Germany : German Materials Society - DGM e. V.
    Data:
    konferencja 03-07 wrzesień, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  13. Study of kesterite Cu2ZnSnS4 nanopowder oxidation by TGA/DTA/MS measurements in the flowing oxygen plus argon (1:4 vol.) gas mixture
    Authors:
    Jerzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2024, tom: 5th International Conference on Nanomaterials, Nanofabrication and Nanocharacterization - NANOMACH 2024, strony: 32), Wydawca: Gebze Technical University oraz Kocaeli University - Turcja
    Data:
    konferencja 18-24 April, 2024
    Status:
    Published
    DOI:
    brak - link to the publication
  14. X-Ray photoelectron spectroscopic insight into oxidation of a range of semiconductor kesterite Cu2ZnSnS4 nanopowders after 6 month-exposure to ambient air
    Authors:
    Jerzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2023, tom: SIPS 2023: sustainability through science & technology, strony: 98), Wydawca: Canada : FLOGEN Stars OUTREACH
    Data:
    konferencja 27 November-1 December, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  15. One month in air-oxygen footprint in synthesis and storage of semiconductor kesterite Cu2ZnSnS4 nanopowders
    Authors:
    Jerzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2023, tom: 4 th International Congress on Advanced Materials Science and Engineering, strony: 183), Wydawca: Vienna : International Science and Technology Conference Institute (ISTCI)
    Data:
    konferencja 17-21 marzec, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  16. Selected Aspects of Oxygen Speciation in Nanopowders of Semiconductor Kesterite Cu2ZnSnS4 Prepared by Mechanochemical Synthesis From Metal Sufide Precursor System
    Authors:
    Honorata Osip, Katarzyna Lejda, Jerzy F. Janik
    Conference:
    Abstracts; https://ieeenap.org/data/IEEE_NAP-2022_Book_of_Abstracts.pdf (rok: 2022, tom: IEEE 12th International Conference Nanomaterials: Applications & Properties" (IEEE NAP-2022), strony: 10nee-16), Wydawca: Silesian University of Technology, IEEE Nanotechnology Council, Sumy State University
    Data:
    konferencja September 11-16, 2022
    Status:
    Published
  17. One month in air-oxygen footprint in synthesis and storage of semiconductor kesterite Cu2ZnSnS4 nanopowders
    Authors:
    Jerzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2023, tom: 4 th International Congress on Advanced Materials Science and Engineering, strony: 183), Wydawca: Vienna : International Science and Technology Conference Institute (ISTCI)
    Data:
    konferencja 17-21 marzec, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  18. Micro-Raman spectroscopy used to follow oxidation in ambient air of semiconductor kesterite Cu2ZnSnS4 nanopowders made by mechanochemically-assisted synthesis route
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Piotr Jeleń
    Conference:
    Book of Abstracts (rok: 2023, tom: International Conference on Materials Science - Materials Oceania 2023 and Engineering, strony: 68), Wydawca: PRISM, Nagoya University, Japan
    Data:
    konferencja 26-29 wrzesień, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  19. Oxygen-bearing species evolved in TGA/DTA/MS experiments for nanopowders of semiconductor kesterite Cu2ZnSnS4 prepared from the {2Cu+Zn+Sn+4S} system
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Janusz Partyka
    Conference:
    Book of abstracts (rok: 2022, tom: 4th World Nanotechnology Summit, strony: str. 34), Wydawca: Phronesis
    Data:
    konferencja 19-20 September 2022
    Status:
    Published
  20. Selected Aspects of Oxygen Speciation in Nanopowders of Semiconductor Kesterite Cu2ZnSnS4 Prepared by Mechanochemical Synthesis From Metal Sufide Precursor System
    Authors:
    Honorata Osip, Katarzyna Lejda, Jerzy F. Janik
    Conference:
    Abstracts; https://ieeenap.org/data/IEEE_NAP-2022_Book_of_Abstracts.pdf (rok: 2022, tom: IEEE 12th International Conference Nanomaterials: Applications & Properties" (IEEE NAP-2022), strony: 10nee-16), Wydawca: Silesian University of Technology, IEEE Nanotechnology Council, Sumy State University
    Data:
    konferencja September 11-16, 2022
    Status:
    Published
  21. Convenient two-step analysis of adventitious surface-bound and bulk oxygen contents in the metal and sulfide precursors to semiconductor kesterite Cu2ZnSnS4
    Authors:
    H. Osip, K. Lejda, M. Drygaś, J.F. Janik
    Conference:
    Book of Astracts - NN21, 18th International Conference on Nanosciences and Nanotechnologies (dostępny po zalogowaniu) (rok: 2021, tom: NN21 - 18th Int. Conf. on Nano, strony: 179), Wydawca: Aristotle University of Thessaloniki, Thessaloniki, Greece
    Data:
    konferencja 6-9 July 2021
    Status:
    Published
  22. Convenient two-step analysis of adventitious surface-bound and bulk oxygen contents in the metal and sulfide precursors to semiconductor kesterite Cu2ZnSnS4
    Authors:
    H. Osip, K. Lejda, M. Drygaś, J.F. Janik
    Conference:
    Book of Astracts - NN21, 18th International Conference on Nanosciences and Nanotechnologies (dostępny po zalogowaniu) (rok: 2021, tom: NN21 - 18th Int. Conf. on Nano, strony: 179), Wydawca: Aristotle University of Thessaloniki, Thessaloniki, Greece
    Data:
    konferencja 6-9 July 2021
    Status:
    Published
  23. Oxygen-bearing species evolved in TGA/DTA/MS experiments for nanopowders of semiconductor kesterite Cu2ZnSnS4 prepared from the {2Cu+Zn+Sn+4S} system
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Janusz Partyka
    Conference:
    Book of abstracts (rok: 2022, tom: 4th World Nanotechnology Summit, strony: str. 34), Wydawca: Phronesis
    Data:
    konferencja 19-20 September 2022
    Status:
    Published
  24. Solid-state 65Cu/119Sn MAS NMR study of prolonged oxidation in ambient air of semiconductor kesterite CuZnSnS4 nanopowders
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Zbigniew Olejniczak
    Conference:
    Book of Abstracts (rok: 2023, tom: SIPS 2023 - sustainability through science & technology, strony: 99), Wydawca: Canada : FLOGEN Stars OUTREACH
    Data:
    konferencja 27 November-1 December, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  25. 6 month-long insight into the oxidation in air of semiconductor Cu2ZnSnS4 nanopowders
    Authors:
    Katarzyna Lejda, Jerzy F. Janik
    Conference:
    Book of Abstracts (rok: 2023, tom: FEMS EUROMAT23 : [materials science and technology in Europe], strony: 1343), Wydawca: Germany : German Materials Society - DGM e. V.
    Data:
    konferencja 03-07 wrzesień, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  26. Micro-Raman spectroscopy used to follow oxidation in ambient air of semiconductor kesterite Cu2ZnSnS4 nanopowders made by mechanochemically-assisted synthesis route
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Piotr Jeleń
    Conference:
    Book of Abstracts (rok: 2023, tom: International Conference on Materials Science - Materials Oceania 2023 and Engineering, strony: 68), Wydawca: PRISM, Nagoya University, Japan
    Data:
    konferencja 26-29 wrzesień, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  27. Effect of kesterite oxidation in the ambient air on its semiconductor properties – study of kesterite nanopowders from three different precursor systems
    Authors:
    Katarzyna Lejda, Jerzy F. Janik
    Conference:
    Book of Abstracts (rok: 2023, tom: FEMS EUROMAT23 : [Materials Science and Technology in Europe], strony: 1355), Wydawca: Germany : German Materials Society - DGM e. V.
    Data:
    konferencja 3-7 wrzesień, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  28. Selected Aspects of Oxygen Speciation in Nanopowders of Semiconductor Kesterite Cu2ZnSnS4 Prepared by Mechanochemical Synthesis From Metal Sufide Precursor System
    Authors:
    Honorata Osip, Katarzyna Lejda, Jerzy F. Janik
    Conference:
    Abstracts; https://ieeenap.org/data/IEEE_NAP-2022_Book_of_Abstracts.pdf (rok: 2022, tom: IEEE 12th International Conference Nanomaterials: Applications & Properties" (IEEE NAP-2022), strony: 10nee-16), Wydawca: Silesian University of Technology, IEEE Nanotechnology Council, Sumy State University
    Data:
    konferencja September 11-16, 2022
    Status:
    Published
  29. Oxygen aspect in high-pressure and high-temperature sintering of nanocrystalline powders of semiconductor kesterite Cu2ZnSnS4
    Authors:
    Jerzy F. Janik, Katarzyna Lejda, Svitlana Stelmakh, Bogdan Palosz
    Conference:
    Book of abstracts (rok: 2022, tom: 4th World Nanotechnology Summit, strony: str. 33), Wydawca: Phronesis
    Data:
    konferencja 19-20 September 2022
    Status:
    Published
  30. X-Ray photoelectron spectroscopic insight into oxidation of a range of semiconductor kesterite Cu2ZnSnS4 nanopowders after 6 month-exposure to ambient air
    Authors:
    Jerzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2023, tom: SIPS 2023: sustainability through science & technology, strony: 98), Wydawca: Canada : FLOGEN Stars OUTREACH
    Data:
    konferencja 27 November-1 December, 2023
    Status:
    Published
    DOI:
    brak - link to the publication
  31. Infrared FT-IR insight into prolonged exposure to ambient air of semiconductor kesterite Cu2ZnSnS4 nanopowders prepared via mechanochemical synthesis route
    Authors:
    Jerzy F. Janik, Katarzyna Lejda
    Conference:
    Book of Abstracts (rok: 2023, tom: International Conference on Materials Science and Engineering - Materials Oceania 2023, strony: 67-68), Wydawca: PRISM, Nagoya University, Japan
    Data:
    konferencja 26-29 wrzesień, 2023
    Status:
    Published
    DOI:
    brak - link to the publication

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