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Multinuclear metal complexes with large macrocycles derived from 2,6-diformylpyridine and trans-1,2-diaminocyclopentane.

2017/25/B/ST5/00722

Keywords

Descriptors

  • ST5_22: Chemia supramolekularna
  • ST5_24: Chemia nieorganiczna
  • ST5_14: Chemia koordynacyjna

Panel

ST5 – Materials: materials synthesis, structure-properties relations, advanced and functional materials with designed properties, (macro)molecular architecture, material engineering

Host institution

Uniwersytet Wrocławski, Wydział Chemii

Voivodeship: dolnośląskie

Other projects carried out by the institution »

Principal investigator (from the host institution)

dr Janusz Stanisław Gregoliński

Number of co-investigators in the project: 5

Call

OPUS 13 – announced on 2017-03-15

Amount awarded
533 300 PLN
Project start date
2018-01-12
Project end date
2022-01-11
Project duration
48 months (the same as in the proposal)
Project status
Project settled

Project description

Download the project description in a pdf file

Note — project descriptions were prepared by the authors of the applications themselves and placed in the system in an unchanged form.

Equipment purchased [PL]

  1. Kolumna preparatywna do chromatografii GPC. Cost: 52 000 PLN
  2. System próżniowy z kontrolą ciśnienia. Cost: 20 000 PLN
  3. Wyparka próżniowa. Cost: 14 000 PLN
  4. Zawór do przełączania kolumn GPC. Cost: 4 500 PLN
  5. Zestaw do woltamperometrii cyklicznej.. Cost: 90 000 PLN
  6. mieszadło magnetyczne. Cost: 7 000 PLN
  7. myjka ultradźwiękowa.
  8. zbiornik Devara. Cost: 7 000 PLN

Information in the final report

Publication in academic press/journals (4)

  1. Monomeric and dimeric nitrate lanthanide(III) and yttrium(III) coordination compounds of (2+2) imine macrocycle derived from 2,6-diformylpyridine and trans-1,2-diaminocyclopentane

    Authors:
    Janusz Gregoliński, Katarzyna Ślepokura
    Academic press:
    polyhedron (year: 2020, volume: 181, pages: 14433/1-114433/13), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.poly.2020.114433 – link to the publication

  2. A New Synthetic Strategy Leading to Homochiral Macrocycles Derived from 2,6-Diformylpyridine and (1S,2S)-trans-1,2- Diaminocyclopentane

    Authors:
    Janusz Gregoliński, Katarzyna Ślepokura, Andrzej Bil, Jerzy Lisowski
    Academic press:
    European Journal of Organic Chemistry (year: 2020, volume: 35, pages: 5714-5728), Publisher: Wiley-VCH GmbH
    Status:
    Published
    DOI:
    10.1002/ejoc.202000919 – link to the publication

  3. Controlling chirality in the synthesis of 4 + 4 diastereomeric amine macrocycles derived from trans-1,2-diaminocyclopentane and 2,6- diformylpyridine

    Authors:
    Dominika Fedorowicz, Sylwia Banach, Patrycja Koza, Rafał Frydrych, Katarzyna Ślepokura Janusz Gregoliński
    Academic press:
    Organic & Biomolecular Chemistry (year: 2022, volume: 20, pages: 1080-1094), Publisher: The Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/d1ob02410h – link to the publication

  4. Mixed macrocycles derived from 2,6-diformylpyridine and opposite enantiomers of trans-1,2-diaminocyclopentane and trans-1,2-diaminocyclohexane.

    Authors:
    Rafał Frydrych, Katarzyna Ślepokura, Andrzej Bil, Janusz Gregoliński
    Academic press:
    Journal of Organic Chemistry (year: 2019, volume: 84, pages: 5695−5711), Publisher: ACS
    Status:
    Published
    DOI:
    10.1021/acs.joc.9b00614 – link to the publication

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