Searching for alternative derivatizing agents for the trace analysis of pharmaceuticals in natural samples using gas chromatography methods

2011/01/N/ST4/02478

Keywords

Descriptors

  • ST4_6: Chemia analityczna
  • ST4_8: Metody instrumentalne w chemii
  • ST4_18: Inne zagadnienia pokrewne

Panel

ST4 – Chemistry: physical chemistry/chemical physics, theoretical chemistry, analytical chemistry, inorganic chemistry, organic chemistry, method development

Host institution

Uniwersytet Gdański

Voivodeship: pomorskie

Other projects carried out by the institution »

Principal investigator (from the host institution)

dr Magda Ewa Caban

Number of co-investigators in the project: 2

Call

PRELUDIUM 1 – announced on 2011-03-15

Amount awarded
149 750 PLN
Project start date
2011-12-13
Project end date
2013-12-12
Project duration
24 months (the same as in the proposal)
Project status
Project settled

Equipment purchased [PL]

  1. Blok grzejny. Cost: 8 000 PLN
  2. Waga analityczna.
  3. Wytrząsarka typu Vortex. Cost: 2 000 PLN

Information in the final report

Publication in academic press/journals (4)

  1. A new silylation reagent dimethyl(3,3,3-trifluoropropyl)silyldiethylamine for the analysis of estrogenic compounds by gas chromatography–mass spectrometry

    Authors:
    Magda Caban, Małgorzata Czerwicka, Paulina Łukaszewicz, Natalia Migowska, Piotr Stepnowski, Marek Kwiatkowski, Jolanta Kumirska
    Academic press:
    Journal of Chromatography A (year: 2013, volume: 1301, pages: 215-224), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.chroma.2013.05.073 – link to the publication
  2. A new silylating reagent – dimethyl(3,3,3-trifluoropropyl)silyldiethylamine – for the derivatisation of non-steroidal anti-inflammatory drugs prior to gas chromatography-mass spectrometry analysis

    Authors:
    Magda Caban, Katarzyna Mioduszewska, Paulina Łukasiewicz, Natalia Migowska, Piotr Stepnowski, Marek Kwiatkowski, Jolanta Kumirska
    Academic press:
    Journal of Chromatography A (year: 2014, volume: 1346, pages: 107–116), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.chroma.2014.04.054 – link to the publication
  3. Determination of pharmaceutical residues in drinking water in Poland using a new SPE-GC-MS(SIM) method based on Speedisk extraction disks and DIMETRIS derivatization

    Authors:
    Magda Caban, Ewa Lis, Jolanta Kumirska, Piotr Stepnowski
    Academic press:
    Science of The Total Environment (year: 2015, volume: 538, pages: 402-411), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.scitotenv.2015.08.076 – link to the publication
  4. Dimethyl(3,3,3-trifluoropropyl)silyldiethylamine—A new silylating agent for the derivatization of β-blockers and β-agonists in environmental samples

    Authors:
    Magda Caban, Katarzyna Mioduszewska, Piotr Stepnowski, Marek Kwiatkowski, Jolanta Kumirska
    Academic press:
    Analityca Chimica Acta (year: 2013, volume: 782, pages: 75-88), Publisher: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.aca.2013.04.018 – link to the publication

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Graphic design and implementation: Jakub Piotrowski