Projects funded by the NCN

Information on the principal investigator and host institution

Information of the project and the call

Keywords

Equipment

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Searching for alternative derivatizing agents for the trace analysis of pharmaceuticals in natural samples using gas chromatography methods

2011/01/N/ST4/02478

Keywords:

beta-blockres beta-agonists antiepileptic drugs gas chromatography derivatization

Descriptors:

  • ST4_6: Instrumental methods in chemistry
  • ST4_8: Organic chemistry
  • ST4_18: Radiation and nuclear chemistry

Panel:

ST4 - Chemistry: physical chemistry/chemical physics, theoretical chemistry, analytical chemistry, inorganic chemistry, organic chemistry, method development

Host institution :

UNIWERSYTET GDAŃSKI

woj. pomorskie

Other projects carried out by the institution 

Principal investigator (from the host institution):

dr Magda Caban 

Number of co-investigators in the project: 2

Call: PRELUDIUM 1 - announced on 2011-03-15

Amount awarded: 149 750 PLN

Project start date (Y-m-d): 2011-12-13

Project end date (Y-m-d): 2013-12-12

Project duration:: 24 months (the same as in the proposal)

Project status: Project settled

Equipment purchased [PL]

  1. Wytrząsarka typu Vortex (2 000 PLN)
  2. Blok grzejny (8 000 PLN)
  3. Waga analityczna.

Information in the final report

  • Publication in academic press/journals (4)
  1. A new silylating reagent – dimethyl(3,3,3-trifluoropropyl)silyldiethylamine – for the derivatisation of non-steroidal anti-inflammatory drugs prior to gas chromatography-mass spectrometry analysis
    Authors:
    Magda Caban, Katarzyna Mioduszewska, Paulina Łukasiewicz, Natalia Migowska, Piotr Stepnowski, Marek Kwiatkowski, Jolanta Kumirska
    Academic press:
    Journal of Chromatography A (rok: 2014, tom: 1346, strony: 107–116), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.chroma.2014.04.054 - link to the publication
  2. Dimethyl(3,3,3-trifluoropropyl)silyldiethylamine—A new silylating agent for the derivatization of β-blockers and β-agonists in environmental samples
    Authors:
    Magda Caban, Katarzyna Mioduszewska, Piotr Stepnowski, Marek Kwiatkowski, Jolanta Kumirska
    Academic press:
    Analityca Chimica Acta (rok: 2013, tom: 782, strony: 75-88), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.aca.2013.04.018 - link to the publication
  3. Determination of pharmaceutical residues in drinking water in Poland using a new SPE-GC-MS(SIM) method based on Speedisk extraction disks and DIMETRIS derivatization
    Authors:
    Magda Caban, Ewa Lis, Jolanta Kumirska, Piotr Stepnowski
    Academic press:
    Science of The Total Environment (rok: 2015, tom: 538, strony: 402-411), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.scitotenv.2015.08.076 - link to the publication
  4. A new silylation reagent dimethyl(3,3,3-trifluoropropyl)silyldiethylamine for the analysis of estrogenic compounds by gas chromatography–mass spectrometry
    Authors:
    Magda Caban, Małgorzata Czerwicka, Paulina Łukaszewicz, Natalia Migowska, Piotr Stepnowski, Marek Kwiatkowski, Jolanta Kumirska
    Academic press:
    Journal of Chromatography A (rok: 2013, tom: 1301, strony: 215-224), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.chroma.2013.05.073 - link to the publication

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