Projects funded by the NCN

Information on the principal investigator and host institution

Information of the project and the call

Keywords

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New strategies of solid state NMR spectroscopy in structural studies of selected bioorganic compounds and functionalized materials

2011/01/B/ST4/02637

Keywords:

Solid State NMR UF MAS NMR Drug Delivery System soft-matter

Descriptors:

  • ST4_3:
  • ST4_4:

Panel:

ST4 - Chemistry: physical chemistry/chemical physics, theoretical chemistry, analytical chemistry, inorganic chemistry, organic chemistry, method development

Host institution :

Centrum Badań Molekularnych i Makromolekularnych Polskiej Akademii Nauk

woj. łódzkie

Other projects carried out by the institution 

Principal investigator (from the host institution):

prof. Marek Józef Potrzebowski 

Number of co-investigators in the project: 8

Call: OPUS 1 - announced on 2011-03-15

Amount awarded: 872 000 PLN

Project start date (Y-m-d): 2011-12-01

Project end date (Y-m-d): 2014-11-30

Project duration:: 36 months (the same as in the proposal)

Project status: Project settled

Equipment purchased [PL]

  1. Sonda (150 000 PLN)
  2. Homogenizator (18 000 PLN)
  3. Liofilizator.
  4. Notebook z oprogramowaniem (12 000 PLN)
  5. Osuszacz powietrza (15 000 PLN)
  6. Wyparka rotacyjna (27 000 PLN)

Information in the final report

  • Publication in academic press/journals (17)
  1. Ibuprofen in Mesopores of Mobil Crystalline Material 41 (MCM-41): A Deeper Understanding
    Authors:
    Ewa Skorupska, Agata Jeziorna, Piotr Paluch, Marek J. Potrzebowski
    Academic press:
    Molecular Pharmaceutics (rok: 2014, tom: 11, strony: 1512-1519), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/mp400670f - link to the publication
  2. NMR Study of BA/FBA Cocrystal Confined Within Mesoporous Silica Nanoparticles Employing Thermal Solid Phase Transformation
    Authors:
    Ewa Skorupska, Piotr Paluch, Agata Jeziorna, Marek J. Potrzebowski
    Academic press:
    The Journal of Physical Chemistry C (rok: 2015, tom: 119, strony: 8625-8661), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp5123008 - link to the publication
  3. Solid State NMR Study of Thermal Processes in Nanoassemblies Formed by Dipeptides
    Authors:
    Magdalena Jaworska, Agata Jeziorna, Ewelina Drabik, Marek J. Potrzebowski
    Academic press:
    The Journal of Physical Chemistry C (rok: 2012, tom: 116, strony: 12330-12338), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp302616n - link to the publication
  4. Recent progress in solid-state NMR studies of drugs confined within drug delivery systems
    Authors:
    Ewa Skorupska, Agata Jeziorna, Slawomir Kazmierski, Marek J. Potrzebowski
    Academic press:
    Solid State Nuclear Magnetic Resonance (rok: 2014, tom: 57-58, strony: 45704), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.ssnmr.2013.12.0 - link to the publication
  5. The comparison of approaches to the solid-state NMR-based structural refinement of vitamin B1 hydrochloride and of its monohydrate
    Authors:
    Jiří Czernek, Tomasz Pawlak, Marek J. Potrzebowski, Jiří Brus
    Academic press:
    Chemical Physics Letters (rok: 2013, tom: 555, strony: 135-140), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.cplett.2012.11.002 - link to the publication
  6. Study of the Mechanism of Thermal Chemical Processes in the Crystals of YAF Tripeptides by Means of Mass Spectrometry and Solid State NMR
    Authors:
    Ewelina Drabik, Agata Jeziorna, Urszula Bienias, Katarzyna Trzeciak-Karlikowska, Tomasz Pawlak, Piotr Paluch, Marek J. Potrzebowski
    Academic press:
    The Journal of Physical Chemistry B (rok: 2013, tom: 117, strony: 13481-13489), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp407080q - link to the publication
  7. Recent Progress in the Solid-State NMR Studies of Short Peptides: Techniques, Structure and Dynamics
    Authors:
    Agata Jeziorna, Slawomir Kazmierski, Piotr Paluch, Ewa Skorupska, Marek J. Potrzebowski
    Academic press:
    Annual Reports on NMR Spectroscopy (rok: 2014, tom: 83, strony: 67-143), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/ - link to the publication
  8. Slow and Very Fast MAS Solid State NMR Study of Biopolymers
    Authors:
    Tomasz Pawlak, Piotr Paluch, Agata Jeziorna, Grzegorz D. Bujacz,Marek J. Potrzebowski
    Academic press:
    Macromolecular Symposia (rok: 2014, tom: 339, strony: 60-69), Wydawca: WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
    Status:
    Published
    DOI:
    10.1002/masy.201300139 - link to the publication
  9. Magic angle spinning NMR study of interaction of N-terminal sequence of dermorphin (Tyr-D -Ala-Phe-Gly) with phospholipids
    Authors:
    Agata Jeziorna, Tomasz Pawlak, Katarzyna Trzeciak-Karlikowska, Piotr Paluch, Marek J. Potrzebowski
    Academic press:
    Biochimica et Biophysica Acta - Biomembranes (rok: 2012, tom: 1818, strony: 2579-2587), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.bbamem.2012.06.013 - link to the publication
  10. Fine refinement of solid state structure of racemic form of phospho-tyrosine employing NMR Crystallography approach
    Authors:
    Piotr Paluch, Tomasz Pawlak, Marcin Oszajca, Wieslaw Lasocha, Marek J. Potrzebowski
    Academic press:
    Solid State Nuclear Magnetic Resonance (rok: 2015, tom: 65, strony: 45699), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.ssnmr.2014.08.002 - link to the publication
  11. Ibuprofen in Mesopores of Mobil Crystalline Material 41 (MCM-41): A Deeper Understanding
    Authors:
    Ewa Skorupska, Agata Jeziorna, Piotr Paluch, Marek J. Potrzebowski
    Academic press:
    Molecular Pharmaceutics (rok: 2014, tom: 11, strony: 1512-1519), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/mp400670f - link to the publication
  12. Study of the Mechanism of Thermal Chemical Processes in the Crystals of YAF Tripeptides by Means of Mass Spectrometry and Solid State NMR
    Authors:
    Ewelina Drabik, Agata Jeziorna, Urszula Bienias, Katarzyna Trzeciak-Karlikowska, Tomasz Pawlak, Piotr Paluch, Marek J. Potrzebowski
    Academic press:
    The Journal of Physical Chemistry B (rok: 2013, tom: 117, strony: 13481-13489), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp407080q - link to the publication
  13. Recent progress in solid-state NMR studies of drugs confined within drug delivery systems
    Authors:
    Ewa Skorupska, Agata Jeziorna, Slawomir Kazmierski, Marek J. Potrzebowski
    Academic press:
    Solid State Nuclear Magnetic Resonance (rok: 2014, tom: 57-58, strony: 45704), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.ssnmr.2013.12.0 - link to the publication
  14. Study of the thermal processes in molecular crystals of peptides by means of NMR crystallography
    Authors:
    Tomasz Pawlak, Piotr Paluch, Katarzyna Trzeciak-Karlikowska, Agata Jeziorna, Marek J. Potrzebowski
    Academic press:
    Crystal Engineering Communications (rok: 2013, tom: 15, strony: 8680-8692), Wydawca: The Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/c3ce40090e - link to the publication
  15. Simple and accurate determination of X–H distances under ultra-fast MAS NMR
    Authors:
    Piotr Paluch, Tomasz Pawlak, Jean-Paul Amoureux, Marek J. Potrzebowski
    Academic press:
    Journal of Magnetic Resonance (rok: 2013, tom: 233, strony: 56-63), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.jmr.2013.05.005 - link to the publication
  16. Solid State NMR Study of Thermal Processes in Nanoassemblies Formed by Dipeptides
    Authors:
    Magdalena Jaworska, Agata Jeziorna, Ewelina Drabik, Marek J. Potrzebowski
    Academic press:
    The Journal of Physical Chemistry C (rok: 2012, tom: 116, strony: 12330-12338), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp302616n - link to the publication
  17. Magic angle spinning NMR study of interaction of N-terminal sequence of dermorphin (Tyr-D -Ala-Phe-Gly) with phospholipids
    Authors:
    Agata Jeziorna, Tomasz Pawlak, Katarzyna Trzeciak-Karlikowska, Piotr Paluch, Marek J. Potrzebowski
    Academic press:
    Biochimica et Biophysica Acta - Biomembranes (rok: 2012, tom: 1818, strony: 2579-2587), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.bbamem.2012.06.013 - link to the publication

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