Projects funded by the NCN


Information on the principal investigator and host institution

Information of the project and the call

Keywords

Equipment

Delete all

New strategies of solid state NMR spectroscopy in structural studies of selected bioorganic compounds and functionalized materials

2011/01/B/ST4/02637

Keywords:

Solid State NMR UF MAS NMR Drug Delivery System soft-matter

Descriptors:

  • ST4_3: Molecular architecture and structure
  • ST4_4: Theoretical and computational chemistry

Panel:

ST4 - Chemistry: physical chemistry/chemical physics, theoretical chemistry, analytical chemistry, inorganic chemistry, organic chemistry, method development

Host institution :

Centrum Badań Molekularnych i Makromolekularnych Polskiej Akademii Nauk

woj. łódzkie

Other projects carried out by the institution 

Principal investigator (from the host institution):

prof. Marek Potrzebowski 

Number of co-investigators in the project: 8

Call: OPUS 1 - announced on 2011-03-15

Amount awarded: 872 000 PLN

Project start date (Y-m-d): 2011-12-01

Project end date (Y-m-d): 2014-11-30

Project duration:: 36 months (the same as in the proposal)

Project status: Project settled

Equipment purchased [PL]

  1. Sonda (150 000 PLN)
  2. Homogenizator (18 000 PLN)
  3. Liofilizator.
  4. Notebook z oprogramowaniem (12 000 PLN)
  5. Osuszacz powietrza (15 000 PLN)
  6. Wyparka rotacyjna (27 000 PLN)

Information in the final report

  • Publication in academic press/journals (12)
  1. Slow and Very Fast MAS Solid State NMR Study of Biopolymers
    Authors:
    Tomasz Pawlak, Piotr Paluch, Agata Jeziorna, Grzegorz D. Bujacz,Marek J. Potrzebowski
    Academic press:
    Macromolecular Symposia (rok: 2014, tom: 339, strony: 60-69), Wydawca: WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
    Status:
    Published
    DOI:
    10.1002/masy.201300139 - link to the publication
  2. NMR Study of BA/FBA Cocrystal Confined Within Mesoporous Silica Nanoparticles Employing Thermal Solid Phase Transformation
    Authors:
    Ewa Skorupska, Piotr Paluch, Agata Jeziorna, Marek J. Potrzebowski
    Academic press:
    The Journal of Physical Chemistry C (rok: 2015, tom: 119, strony: 8625-8661), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp5123008 - link to the publication
  3. Recent progress in solid-state NMR studies of drugs confined within drug delivery systems
    Authors:
    Ewa Skorupska, Agata Jeziorna, Slawomir Kazmierski, Marek J. Potrzebowski
    Academic press:
    Solid State Nuclear Magnetic Resonance (rok: 2014, tom: 57-58, strony: 45338), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.ssnmr.2013.12.0 - link to the publication
  4. Study of the Mechanism of Thermal Chemical Processes in the Crystals of YAF Tripeptides by Means of Mass Spectrometry and Solid State NMR
    Authors:
    Ewelina Drabik, Agata Jeziorna, Urszula Bienias, Katarzyna Trzeciak-Karlikowska, Tomasz Pawlak, Piotr Paluch, Marek J. Potrzebowski
    Academic press:
    The Journal of Physical Chemistry B (rok: 2013, tom: 117, strony: 13481-13489), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp407080q - link to the publication
  5. Ibuprofen in Mesopores of Mobil Crystalline Material 41 (MCM-41): A Deeper Understanding
    Authors:
    Ewa Skorupska, Agata Jeziorna, Piotr Paluch, Marek J. Potrzebowski
    Academic press:
    Molecular Pharmaceutics (rok: 2014, tom: 11, strony: 1512-1519), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/mp400670f - link to the publication
  6. Simple and accurate determination of X–H distances under ultra-fast MAS NMR
    Authors:
    Piotr Paluch, Tomasz Pawlak, Jean-Paul Amoureux, Marek J. Potrzebowski
    Academic press:
    Journal of Magnetic Resonance (rok: 2013, tom: 233, strony: 56-63), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.jmr.2013.05.005 - link to the publication
  7. Solid State NMR Study of Thermal Processes in Nanoassemblies Formed by Dipeptides
    Authors:
    Magdalena Jaworska, Agata Jeziorna, Ewelina Drabik, Marek J. Potrzebowski
    Academic press:
    The Journal of Physical Chemistry C (rok: 2012, tom: 116, strony: 12330-12338), Wydawca: ACS Publications
    Status:
    Published
    DOI:
    10.1021/jp302616n - link to the publication
  8. Study of the thermal processes in molecular crystals of peptides by means of NMR crystallography
    Authors:
    Tomasz Pawlak, Piotr Paluch, Katarzyna Trzeciak-Karlikowska, Agata Jeziorna, Marek J. Potrzebowski
    Academic press:
    Crystal Engineering Communications (rok: 2013, tom: 15, strony: 8680-8692), Wydawca: The Royal Society of Chemistry
    Status:
    Published
    DOI:
    10.1039/c3ce40090e - link to the publication
  9. Fine refinement of solid state structure of racemic form of phospho-tyrosine employing NMR Crystallography approach
    Authors:
    Piotr Paluch, Tomasz Pawlak, Marcin Oszajca, Wieslaw Lasocha, Marek J. Potrzebowski
    Academic press:
    Solid State Nuclear Magnetic Resonance (rok: 2015, tom: 65, strony: 45333), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.ssnmr.2014.08.002 - link to the publication
  10. Magic angle spinning NMR study of interaction of N-terminal sequence of dermorphin (Tyr-D -Ala-Phe-Gly) with phospholipids
    Authors:
    Agata Jeziorna, Tomasz Pawlak, Katarzyna Trzeciak-Karlikowska, Piotr Paluch, Marek J. Potrzebowski
    Academic press:
    Biochimica et Biophysica Acta - Biomembranes (rok: 2012, tom: 1818, strony: 2579-2587), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.bbamem.2012.06.013 - link to the publication
  11. Recent Progress in the Solid-State NMR Studies of Short Peptides: Techniques, Structure and Dynamics
    Authors:
    Agata Jeziorna, Slawomir Kazmierski, Piotr Paluch, Ewa Skorupska, Marek J. Potrzebowski
    Academic press:
    Annual Reports on NMR Spectroscopy (rok: 2014, tom: 83, strony: 67-143), Wydawca: Elsevier
    Status:
    Published
  12. The comparison of approaches to the solid-state NMR-based structural refinement of vitamin B1 hydrochloride and of its monohydrate
    Authors:
    Jiří Czernek, Tomasz Pawlak, Marek J. Potrzebowski, Jiří Brus
    Academic press:
    Chemical Physics Letters (rok: 2013, tom: 555, strony: 135-140), Wydawca: Elsevier
    Status:
    Published
    DOI:
    10.1016/j.cplett.2012.11.002 - link to the publication